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麋鹿迷路

金虫 (小有名气)

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虫号: 781590
注册: 2009-05-28
专业: 聚合物共混与复合材料

[交流] 如何根据审稿人意见改稿

去年年底投的，是研究生期间的第一篇，春节前收到了审稿人意见，现在老板催了，但还有很多问题我不知道要怎么答和修改，请各位虫子帮帮忙，帮我看下要怎么改，谢谢。

Reviewer #1:
1 1. In introduction, authors explain that a)water preferentially permeates through hydrophilic membrane b)APTEOS controls swelling of PVA meanwhile the amino groups of APTEOS have strong interaction with water and form a pre-separation layer suggesting that water permselectivity will increase. It could be concluded that water permselectivity increases by increasing hydrophilicity only.
page 9 line 16-17, results of authors show the opposite: the water permselectivity increases with contact angle increase indicating that the surface becomes less hydrophilic after APTEOS treatment.
I suggest that the authors clarify the relation between hydrophilicity and permselectivity in this case.
理论上APTEOS加入后NH2基团是可以增加水的通量，接触角实验我每个样做了至少15次，但结果是量越多，接触角越大，我现在有点不明白要怎么阐明亲水性和通量间的关系。

2 聚合物薄膜的厚度用什么测量比较好？我在表面加的东西的厚度怎么确定（大概只有2，3个微米）？

3 另外还想请教一个问题，聚合物XRD上的结晶峰变小可以说是无定形区的压缩吗？还是与结晶区有关？

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