24小时热门版块排行榜    

查看: 180  |  回复: 1
当前主题已经存档。

linglin0409

铜虫 (初入文坛)

[交流] 求助:翻译一段英文文献,急急急!

l-(2-Hydroxyethyl)-3-(l,2,3,4-tetrahydro-2,4-dioxo-5-pyrimidinyl)
urea (VII). Method B.—A mixture of 1-methyl-l-nitroso-
3-(l,2,3,4-tetrahydro-2,4-dioxo-5-pyrimidinyl)urea (4.60 g.,0.0216 mole), 2-aminoethanol (1.27 ml., 0.0216 mole), and water(100 ml.) was heated under reflux for 2 hr. The reaction mixture diluted with water (1 1.) was heated to boiling, and a small amount of insoluble material was removed by filtration.The white solid deposited in the filtrate after two days at room temperature was washed with water and dried in vacuo  at 100° overnight; yield of VII, 2.4 g. (52%)
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

yjhorn

木虫 (正式写手)

★ ★ ★ ★ ★ ★ ★ ★
linglin0409(金币+3,VIP+0): 11-14 14:00
zap65535(金币+5,VIP+0):补发 12-22 03:03
l-(2-羟乙基)-3-(l,2,3,4-四氢-2,4-双氧-5-嘧啶)尿素(VII).

方法B:1-甲基-l-亚硝基-3-(l,2,3,4-四氢-2,4-双氧-5-嘧啶)尿素,2-氨基乙醇和水的混合液加热回流2h。用水稀释该溶液,加热至沸腾,过滤除去小量不溶物质。将滤液放置室温两天,白色固体析出,沉积。用水冲洗白色固体,然后100度真空干燥过夜,产生VII 2.4G,产率为52%。
认识大家是缘分啊!
2楼2009-11-14 13:21:30
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖
相关版块跳转 我要订阅楼主 linglin0409 的主题更新
普通表情 高级回复(可上传附件)
信息提示
请填处理意见