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liuxianlin
铁杆木虫 (职业作家)
- 博学EPI: 1
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- 金币: 11324.5
- 散金: 10
- 红花: 3
- 帖子: 3381
- 在线: 231.9小时
- 虫号: 666035
- 注册: 2008-12-01
- 性别: GG
- 专业: 应用有机化学
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Registry Number: 18030-58-5 _ Formula: C12 H8 Cl2 Si CA Index Name: 9H-9-Silafluorene, 9,9-dichloro- Other Names: 5H-Dibenzosilole, 5,5-dichloro- (8CI); Dibenzosilole, 5,5-dichloro- (6CI); 5,5-Dichlorodibenzosilole; 9,9-Dichloro-9-silafluorene; 9,9-Dichloro-9H-9-silafluorene; 9,9-Dichlorosilafluorene; Silaflurenyl dichloride Property Value Condition Boiling Point 176-177 ℃ Press: 16 Torr Boiling Point 155 ℃ Press: 3 Torr Boiling Point 132-134℃ Press: 2 Torr Boiling Point 90-110 ℃ Press: 0.1 Torr Mass Spectrum See full text Mass Spectrum See full text Melting Point 98 ℃ Solv: hexane Melting Point 97-98 ℃ Proton NMR Spectrum See full text Property Value Condition Boiling Point 329.5℃ press: 760 Torr Carbon-13 NMR See spectrum Density 1.32?.1 g/cm3 Temp: 20 ℃ Press: 760 Torr Enthalpy of 54.93?.0 kJ/mol Press: 760 Torr Vaporization Flash Point 145.2-4.3 ℃ Molar Volume 189.5 cm3/mol Temp: 20 ℃ Press: 760 Torr Molecular Weight 251.18 Polar Surface Area 0.00 A2 Vapor Pressure 3.38E-4 Torr Temp: 25 ℃ [ Last edited by liuxianlin on 2009-11-12 at 07:58 ] |
2楼2009-11-12 07:43:40
liuxianlin
铁杆木虫 (职业作家)
- 博学EPI: 1
- 应助: 0 (幼儿园)
- 金币: 11324.5
- 散金: 10
- 红花: 3
- 帖子: 3381
- 在线: 231.9小时
- 虫号: 666035
- 注册: 2008-12-01
- 性别: GG
- 专业: 应用有机化学
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张胜兰(金币+10,VIP+0):非常感谢提供的信息，但下面的文献好多都没有链接，请问能找到嘛？ 11-12 10:36
张胜兰(金币+10,VIP+0):非常感谢提供的信息，但下面的文献好多都没有链接，请问能找到嘛？ 11-12 10:36
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1. Novel fluorene-based biphenolic monomer: 9,9-bis(4-hydroxyphenyl)-9-silafluorene. Seesukphronrarak, Surasak; Takata, Toshikazu. Department of Organic and Polymeric Materials, Tokyo Institute of Technology, Ookayama, Meguro-ku, Tokyo, Japan. Chemistry Letters (2007), 36(9), 1138-1139. Publisher: Chemical Society of Japan, CODEN: CMLTAG ISSN: 0366-7022. Journal written in English 2. Structure and Chemistry of 1-Silafluorenyl Dianion, Its Derivatives, and an Organosilicon Diradical Dianion. Liu, Yuxia; Stringfellow, Thomas C.; Ballweg, David; Guzei, Ilia A.; West, Robert. Organosilicon Research Center Department of Chemistry, University of Wisconsin, Madison, WI, USA. Journal of the American Chemical Society (2002), 124(1), 49-57. Publisher: American Chemical Society, CODEN: JACSAT ISSN: 0002-7863. Journal written in English. http://d.namipan.com/d/2b650a99b ... 069d3393493d34a0300 3. Organosilicon heterocycles. LX. Unsaturated heterocycles containing silicon and oxygen as potential sources of dichlorosilanone. Chernyshev, E. A.; Krasnova, T. L.; Mudrova, N. A.; Bochkarev, V. N. Gos. Nauchno-Issled. Inst. Khim. Tekhnol. Elementoorg. Soedin., Moscow, Russia. Zhurnal Obshchei Khimii (1992), 62(8), 1828-37. CODEN: ZOKHA4 ISSN: 0044-460X. Journal written in Russian. 4. Tricyclic heterocycles with bifunctional silicon centers. Corey, Joyce Y.; John Christy S.; Ohmsted, Martha C.; Chang, Lihsueh S. Dep. Chem., Univ. Missouri, St. Louis, MO, USA. Journal of Organometallic Chemistry (1986), 304(1-2), 93-105. CODEN: JORCAI ISSN: 0022-328X. Journal written in English. 5. Silicon-containing heterocyclic compounds. XLV. Novel high-temperature heterocyclization of arylchlorosilanes in the presence of halo-substituted alkanes and alkenes. Chernyshov, E. A.; Komalenkova, N. G.; Shamshin, L. N.; Shashkov, I. A. Gos. Nauchno-Issled. Inst. Khim. Tekhnol. Elementoorg. Soedin., Moscow, USSR. Zhurnal Obshchei Khimii (1985), 55(10), 2317-23. CODEN: ZOKHA4 ISSN: 0044-460X. Journal written in Russian. 6. Silicon-containing heterocyclic compounds. XLIII. Novel intramolecular thermal cyclization involving dichlorosilylene. Chernyshev, E. A.; Komalenkova, N. G.; Bashkirova, S. A.; Shamshin, L. N.; Mosin, A. M. Gos. Nauchno-Issled. Inst. Khim. Tekhnol. Elementoorg. Soedin., Moscow, USSR. Zhurnal Obshchei Khimii (1985), 55(10), 2309-14. CODEN: ZOKHA4 ISSN: 0044-460X. Journal written in Russian. 7. Silicon-containing heterocyclic compounds. XLIV. Synthesis of 9,9-dichloro-9-silafluorene by thermal reaction of o-chlorobiphenyl with hexachlorodisilane. Chernyshev, E. A.; Komalenkova, N. G.; Elagina, O. V.; Rogachevskii, V. L.; Bashkirova, S. A.; Dunaeva, L. V. Gos. Nauchno-Issled. Inst. Khim. Tekhnol. Elementoorg. Soedin., Moscow, USSR. Zhurnal Obshchei Khimii (1985), 55(10), 2314-17. CODEN: ZOKHA4 ISSN: 0044-460X. Journal written in Russian. [ Last edited by liuxianlin on 2009-11-12 at 08:15 ] |
3楼2009-11-12 08:04:01
liuxianlin
铁杆木虫 (职业作家)
- 博学EPI: 1
- 应助: 0 (幼儿园)
- 金币: 11324.5
- 散金: 10
- 红花: 3
- 帖子: 3381
- 在线: 231.9小时
- 虫号: 666035
- 注册: 2008-12-01
- 性别: GG
- 专业: 应用有机化学
4楼2009-11-13 07:49:07