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AQY is reported and SCC, but the procedures lack key metrological details: bandpass (FWHM), spectral irradiance at the reactor, photon flux calibration (e.g., ferrioxalate actinometry), optical geometry (path length, reactor albedo), and inner-filter effects in turbid slurries. Please provide calibrated photon flux at each wavelength at the sample plane, scattering correction, and the method for absorbed-photon-to-chemical efficiency (APCE). The SCC input power uses 0.314 W from 1000 W·m-2×3.14×10-4 m2 (a 1-cm-diameter spot) for a 120 mL slurry with 200 mg catalyst—this geometry likely underestimates incident power on the illuminated volume or overestimates absorption. Please show the illuminated area, light footprint mapping on the reactor, and sensitivity of SCC to stirrer speed/optical depth. 有哪位大神能帮我解释一下审稿人问的到底是啥不？都不知道咋回复 |
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