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ÑõÆøÓëѪºìµ°°×½áºÏ³£ÊýµÄ²âÁ¿Óõ½ÁËÒ»ÖÖÉ豸flow-flash apparatus £¬ÒòΪ¿´µÄÊÇÓ¢ÎÄÎÄÏ×£¬²»Ì«Çå³þÉ豸flow-flash apparatus µ½µ×ÊÇʲôÑùµÄ£¿ÄÄÀïÓÐÂô£¿Ï£ÍûÖªµÀµÄºÃÐÄÈËÄܰï°ïÎÒ£¬Ð»Ð»´ó¼ÒÀ² ¸½ÉÏÓ¢ÎÄÔÎĽéÉÜ£º A brief description of the current flow-flash apparatus is as follows.The reservoirs for reactants were glass cylinders of 5-ml capacity equipped with the inlet and outlet for gases at the top. The solutions were stirred with magnetic stirrers installed in the bottom. The reactant solutions were transferred to horizontal drive syringes by pulling a rod block to which were attached the plungers, and then forced to pass through a jet mixer into an observation tube by a stroke of a pneumatic piston (4.0 kg/cm2). Both reservoirs and drive syringes were mounted in a thermostated aluminum block. The volume of reactant required for one shot was 260 l for each reservoir. The observation cell was fabricated from a block of glass ceramics. A hole 2 mm in diameter was drilled and the two ends were sealed with quartz windows (10 mm apart). The top half of the block was removed by cutting horizontally through the middle of the hole leaving a rectangular opening (2 X 8.5 mrn), which was covered with a quartz window to receive the photolyzing beam. |
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