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twenty3

应助: (幼儿园)
在线:
虫号: 673280

[交流] 【求助】两次XRD的Scan Step Time不一样，如何统一？

一系列的样品，分两次定性测定，而两次的测定条件不一样（主要是步长与每步扫描时间不同），想用数据处理方法将两次结果统一起来，放在一张图中，请问有什么方法？
具体扫描条件：
第一次：------------------------------
Scan Axis: Gonio
Start Position [°2Th.]: 5.3640
End Position [°2Th.]: 99.6660
Step Size [°2Th.]: 0.2340
Scan Step Time [s]: 34.6550
Scan Type: Continuous
PSD Mode: Scanning
PSD Length [°2Th.]: 2.12
Offset [°2Th.]: 0.0000
Divergence Slit Type: Fixed
Divergence Slit Size [°]: 0.9570
Specimen Length [mm]: 10.00
Measurement Temperature [°C]: 25.00
Anode Material: Cu
K-Alpha1 [臸: 1.54060
K-Alpha2 [臸: 1.54443
K-Beta [臸: 1.39225
K-A2 / K-A1 Ratio: 0.50000
Generator Settings: 40 mA, 40 kV
Goniometer Radius [mm]: 240.00
Dist. Focus-Diverg. Slit [mm]: 91.00
Incident Beam Monochromator: No
Spinning: No
第二次：------------------------------
Scan Axis Gonio
Start Position [°2Th.] 5.0418
End Position [°2Th.] 79.9698
Step Size [°2Th.] 0.0840
Scan Step Time [s] 9.8900
Scan Type Continuous
PSD Mode Scanning
PSD Length [°2Th.] 2.12
Offset [°2Th.] 0.0000
Divergence Slit Type Fixed
Divergence Slit Size [°] 0.9570
Specimen Length [mm] 10.00
Measurement Temperature [°C] 25.00
Anode Material Cu
K-Alpha1 [臸 1.54060
K-Alpha2 [臸 1.54443
K-Beta [臸 1.39225
K-A2 / K-A1 Ratio 0.50000
Generator Settings 40 mA, 40 kV
Goniometer Radius [mm] 240.00
Dist. Focus-Diverg. Slit [mm] 91.00
Incident Beam Monochromator No
Spinning No

[ Last edited by twenty3 on 2009-10-20 at 10:50 ]

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