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| The insoluble salt was removed by filtration and the solvent was stripped from the filtrate. Additional salt was removed after addition of ether. The product was distilled as a colorless oil, bp 73¡ã-75¡æ. (9.17 mm). Some white solid co-distilled and was separated by decantation. |
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3Â¥2009-10-19 15:59:29
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