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hongwei.ch

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clearsky7228

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hongwei.ch(½ð±Ò+12,VIP+0):лл 10-19 21:56
sirljz(½ð±Ò+2):лл½»Á÷ 2010-04-01 12:23
1. To a further illustration , A of the blends was extracted with THF, and after extraction the infrared spectra of blends was shown in Figure X. Blends after the extraction almost did not contain A,i.e. it was  clear that there was no or a small amount of reaction in the system , thus it is confirmed that the changes shown in Figure 1  should come from the degradation of the system.

2. In view of  the amount of  benzene ring in PS in the experiment process was constant, so when the absorption peak at 815 wave number (corresponding to the facing 2  replaced the benzene ring) as the base,and  to observe the strengh of absorption peak at 1310  finding that the peak strengh of mechanical  blend was significantly lower compared to the that of solution blends , thus proving the existence of chemical interaction in the system through melt processing.
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cup_fjw

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hongwei.ch(½ð±Ò+2,VIP+0): 10-19 21:56
sirljz(½ð±Ò+1):лл½»Á÷ 2010-04-01 12:24
For further illustration,A was extracted from the blend with THF, XRD of the remainder was shown in Figure X.which revealed that  little A was included in the blend,that meaned no or few reactions took place in the system.so the change shown in Figure 1 was due to the degradation of the system.
2Â¥2009-10-17 09:55:08
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