24小时热门版块排行榜    

Znn3bq.jpeg
查看: 196  |  回复: 1
当前主题已经存档。

slyang8682

铜虫 (初入文坛)

[交流] 【求助】透析实验怎么做?

150ml of the nanoribbon solution was covered by a 5-mm layer of silicon oil in an Erlenmeyer flask. To this solution we added 150ml of concentrated NH4OH (2.22mmol), followed by 150ml of N2H4.H2O(98%,3.03mmol). The oil was added to eliminate the air–water interface that causes agglomeration of the reduced ribbons as water evaporates. The reaction mixture was heated at 95C for 1h in a gently boiling wate rbath (nostirring) .Excess N2H4 was removed by dialysis (CelluSep H1 regenerated cellulose tubular membrane; nominal molecular weight, 5,000 (relative molecular mass); 400-mm width) for 24h in 1% NH4OH. Filtering and drying in vacuo afforded 23.2mg of reduced nanoribbons.

请问各位大侠Excess N2H4 was removed by dialysis (CelluSep H1 regenerated cellulose tubular membrane;nominal molecular weight, 5,000 (relative molecular mass); 400-mm width) for 24h in 1% NH4OH. 所说的透析具体是怎么做的,具体用的是什么膜,都要什么设备。鄙人不是学化学的,什么都不会。谢谢!
回复此楼
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

骑着蜗牛追火箭

木虫 (著名写手)

纳米小生

★ ★
小木虫(金币+0.5):给个红包,谢谢回帖交流
chemistryer(金币+1,VIP+0):鼓励交流 9-19 21:36
一个透析袋,一个大烧杯就可以了。只要你明白透析的原理,就知道怎么做了
2楼2009-09-19 09:06:57
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖
相关版块跳转 我要订阅楼主 slyang8682 的主题更新
普通表情 高级回复 (可上传附件)
最具人气热帖推荐 [查看全部] 作者 回/看 最后发表
[考研] 一志愿厦大0856,306求调剂 +6 Bblinging 2026-04-11 6/300 2026-04-11 14:55 by may_新宇
[考研] 289求调剂 +5 L1ttleTiger 2026-04-04 5/250 2026-04-11 10:47 by zhq0425
[考研] 0854调剂 +8 950824he@ 2026-04-09 8/400 2026-04-11 10:11 by zhq0425
[考研] 293求调剂 +5 勇远库爱314 2026-04-06 5/250 2026-04-11 09:44 by zhq0425
[考研] 一志愿北理工298英一数二已上岸,感谢各位老师 +14 Reframe 2026-04-10 16/800 2026-04-10 23:07 by caotw2020
[考研] 一志愿华南理工大学331分材料求调剂 +9 天下ww 2026-04-09 9/450 2026-04-10 22:58 by Ftglcn90
[考研] 考研调剂 +26 硕星赴 2026-04-09 27/1350 2026-04-10 22:24 by 猪会飞
[考研] 求调剂 +16 MAX怅惘 2026-04-09 18/900 2026-04-10 20:24 by 小鬼喔~~
[考研] 285求调剂 +9 AZMK 2026-04-07 11/550 2026-04-10 15:24 by AZMK
[考研] 一志愿211,化学学硕,310分,本科重点双非,求调剂 +27 努力奋斗112 2026-04-07 30/1500 2026-04-10 15:06 by Kilig0317
[考研] 求调剂 +11 翩翩一书生 2026-04-09 13/650 2026-04-10 10:27 by liuhuiying09
[考研] 生物与医药273求调剂 +18 荔题南墙 2026-04-05 19/950 2026-04-10 08:14 by kangsm
[考研] 已调剂 +18 柴郡猫_ 2026-04-09 19/950 2026-04-09 22:10 by 柴郡猫_
[考研] 311求调剂 +6 surte 2026-04-08 13/650 2026-04-09 14:00 by surte
[考研] 0860004 求调剂 309分 +6 Yin DY 2026-04-09 6/300 2026-04-09 10:19 by 啊李999
[考研] 22408 266求调剂 +11 masss11222 2026-04-07 14/700 2026-04-08 11:06 by yulian1987
[考研] 307求调剂 +3 Youth@@ 2026-04-07 3/150 2026-04-07 09:25 by 小黑不怕难
[考研] 346分的生物与医药08600求调剂 +6 常雨阳上岸 2026-04-05 7/350 2026-04-06 12:36 by lys0704
[考研] 332求调剂 +17 小小孟... 2026-04-05 18/900 2026-04-06 09:51 by 蓝云思雨
[考研] 358求调剂 +7 秋gk 2026-04-04 7/350 2026-04-05 13:29 by huangmoli
信息提示
请填处理意见