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机械虫996

新虫 (正式写手)

[求助] 纳米级的纤维素晶体悬浮液

纳米级的纤维素悬浮液怎么才能得到纤维素?
离心加透析?
透析需要哪些仪器耗材,怎么操作?

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潘凯波bobo

金虫 (正式写手)

你说的后面的那个纤维素,是指单个纤维素分子吗?透析用透析袋就行,可以有不同分子量的,用于蛋白的纯化,一般是小分子出去,蛋白留袋子里。透纤维素我没见过,如果你有看到相关文献,可以分享分享

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2楼2023-02-13 16:55:14
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机械虫996

新虫 (正式写手)

引用回帖:
2楼: Originally posted by 潘凯波bobo at 2023-02-13 16:55:14
你说的后面的那个纤维素,是指单个纤维素分子吗?透析用透析袋就行,可以有不同分子量的,用于蛋白的纯化,一般是小分子出去,蛋白留袋子里。透纤维素我没见过,如果你有看到相关文献,可以分享分享
...

The linter was ground in a Wiley mill and hydrolyzed without any chemical pretreatment. The method of acidic hydrolysis was applied with minor adaptations. The linter was mechanically stirred at a ratio of 1:20 (w/v) of aqueous concentrated sulfuric acid (60%, w/w) with a Teflon?bar dispersing element, at 45?°C, for 60?min. The nanowhiskers suspension was centrifuged for 15?min at 13,000?rpm in a High-speed Refrigerated Centrifuge CR22GIII, and the precipitate was resuspended in distilled water and dialyzed with tap water until a pH (6–7) was reached. The process from centrifugation through dialysis was repeated three times.
棉绒在Wiley磨机中研磨,并在没有任何化学预处理的情况下水解。酸性水解方法(Cranston和Gray,2006,Medeiros等人,2008,Orts等人,2005)经过轻微调整。 将棉绒以1:20(w / v)与特氟龙棒分散元件的比例在60°C下机械搅拌45分钟。将纳米晶须悬浮液在高速冷冻离心机CR60GIII中以13000rpm离心15分钟,并将沉淀物重悬于蒸馏水中并用自来水透析直至达到pH(6-7)。从离心到透析的过程重复三次。

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3楼2023-02-13 17:14:54
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机械虫996

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引用回帖:
2楼: Originally posted by 潘凯波bobo at 2023-02-13 16:55:14
你说的后面的那个纤维素,是指单个纤维素分子吗?透析用透析袋就行,可以有不同分子量的,用于蛋白的纯化,一般是小分子出去,蛋白留袋子里。透纤维素我没见过,如果你有看到相关文献,可以分享分享
...

文献名称:Extraction and characterization of nanocellulose structures from raw cotton linter

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4楼2023-02-13 17:16:12
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机械虫996

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5楼2023-02-15 10:16:46
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