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lixiaod001
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ygb7086(½ð±Ò+5,VIP+0):лл 9-13 08:14
ygb7086(½ð±Ò+5,VIP+0):лл 9-13 08:14
|
£¨Èí¼þ·Ò룩 Photocatalytic degradation experiment of methylene blue in early may at two o 'clock in the afternoon sun, sun, outdoor lighting (no cover). Process is as follows: will Sb2S3 g into 1/4 cup with 100 mL (10 mg/L) methylene blue reaction containers, the solution of ultrasonic dispersing 15 min, and avoid light dark magnetic-driving adsorption, 1 h degradants adsorption equilibrium catalyst in the surface to, VIS - 72 type spectrophotometer test its absorbency and as the initial solution by degradants absorbency A0. Then put in the sunlight, photocatalytic experiments on magnetic mixing, regular sampling, centrifugal separation, take upper solution of methylene blue in the maximum absorption wavelength (lambda Max = 664 nm) in the determination of value A sample, the degradation rate calculated according to the next type X X = (A0 - Ax) / A0 by 100 % [20], type: A0 to decompose methylene blue light before the value, For the sun shine after decomposition Ax methylene blue light absorption solution. |
3Â¥2009-09-12 09:07:40
jw227
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ygb7086(½ð±Ò+25,VIP+0): 9-13 08:14
ygb7086(½ð±Ò+25,VIP+0): 9-13 08:14
| Photocatalytic degradation of methylene blue experiments adopted the sunlight at two in the afternoon of early May as the light source (outdoor, unsheltered sunlight). The process is as follows: The Sb2S3 (0.25 g ) was added to in the reaction container of methylene blue solution 100 mL (10 mg / L), ultrasonic dispersion for 15 min, and then magnetic stirring for 1 h in the dark. After degradation products reached adsorption equilibrium on the catalyst surface, the absorbance was analyzed with the VIS-7200 spectrophotometer as the initial absorbance of degradation products, A0. Subsequently, photocatalytic experiments carried out in sunlight with magnetic stirring and regular sampling. After centrifuged, the absorbance (A) of the supernatant of methylene blue was tested at the maximum absorption wavelength (¦Ëmax = 664 nm) . The degradation rate ( X ) was calculated in accordance with the following formula: X = (A0 - Ax) / A0 ¡Á 100% [20], where A0 is the absorbance of methylene blue before light decomposition; Ax is the absorbance of methylene blue after light decomposition. |

2Â¥2009-09-11 16:49:15














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