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[求助]
有人懂反相微乳液法，求帮助。。
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Two reverse microemulsions with ω (mole ratio between water and surfactant [CO520 and Triton X-100)] = 5.8 were fabricated by individually adding 75 μL of FeCl3 (527.6 × 10−3 m) aqueous solution or 75 μL of DSCP (527.6 × 10−3 m) aqueous solution into 2.5 mL cyclohexane solution containing 0.03 m CO520/0.26 m Triton X-100/1.14 m 1-hexanol under vigorous stirring. Additionally, 10 μL triethylamine (TEA) was added into the mixed microemulsion for further 10 min stirring. After adding ethanol as emulsion breaker, Fe-DSCP NCP nanoparticles were deposited and collected by centrifugation. The obtained Fe-DSCP nanoparticles were washed with ethanol to purification. 以上是文献的方法，我遇见的问题是，DSCP很难溶解，并且文献里反应时间什么的不太明确，破乳加的乙醇量也不知道，感觉无从下手，有懂的大神可以提示一二吗？ 万分感谢！ |
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2楼2021-10-05 17:10:49
