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[交流] DittmerLester钼蓝显色剂配法

我在做磷脂的TLC，显色剂需要DittmerLester钼蓝显色剂，之前按照别人帮忙搜到的配方：
Molybdenum blue reaction according to Dittmer and Lester
For detection of phospholipids and phosphoric acid derivatives
Solution I: Boil 40.11g MoO3 in 1 liter 25N sulfuric acid for 3-4 hours until the molybdenum oxide is completely dissolved. Let the light yellow solution slowly cool to ambient temperature overnight. The solution will turn light blue.
Solution II: Boil 1.78 g molybdenum powder and 500ml of solution I for 15min, cool and decant from the remaining residue.

For preparation of the spray reagent, add equal volumes of solutions I and II to 4.5 volume parts water. A dark green solution is formed.
Solutions I and II are stable for several months when stored in the dark. The spray reagent has to be prepared weekly.

发现三氧化钼根本无法溶解，不知道是不是配方有问题，大家有没有做过相关研究的，给点建议吧，谢谢

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