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xiuhua

铜虫 (小有名气)

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rjw999

银虫 (著名写手)

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xiuhua(金币+1,VIP+0):谢谢 6-9 15:35
我在溶剂手册上查阅到:1,2-二氯乙烷在精制时,用稀氢氧化钠或氢氧化钾溶液洗涤后,再水洗,干燥,蒸馏!干燥剂可用氯化钙,无水硫酸钠,五氧化二磷和分子筛等。强酸强碱会发生反应,故不宜做干燥剂!
厚德正生,臻于至善!!!
8楼2009-06-09 15:09:58
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holycow

木虫 (小有名气)

编辑掉,注意千万别往里面加钠,据说会爆炸

[ Last edited by holycow on 2009-6-10 at 14:19 ]
2楼2009-06-09 10:53:13
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527246736

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xiuhua(金币+1,VIP+0):谢谢 6-9 15:36
Shaken with conc H2SO4 (to remove alcohol added as an oxidation inhibitor), washed with water, then dilute
KOH or aqueous Na2C03 and again with water. After an initial drying with CaC12, MgSO4 or by distn, it is
refluxed with P2O5, Cas04 or CaH2 and fractionally distd. Carbonyl-containing impurities can be removed as
described for chloroform.

It is form Purification of Laborarory Chemicais
3楼2009-06-09 11:01:04
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yangjianchun

木虫 (著名写手)

加入五氧化二磷。。。蒸馏

见溶剂手册p207
越把事当事越是事!
4楼2009-06-09 11:16:48
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