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1.Electrochemical tests were performed on as-deposited thin films on nickel substrates which were cycled between 1.10 and 0.05 V vs. a lithium reference electrode. The two electrodes were separated by a glass filter paper wetted with a standard LiPF6 electrolyte dissolved in a 1:1 mixture of ethylene carbonate and dimethyl carbonate (Merck). 2.The mixture was stirred for 2 h, left to stand at 20¡æfor 24 h, heated at 80¡æ for a further 24 h and finally left in a vacuum oven at 130¡æ for 2 h. The resulting composite was then manually milled to the powder form. |
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