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sunnyyang09

捐助贵宾 (小有名气)

[求助] 谱析TU-1810和PE Lambda 25紫外可见光谱仪,想配50微升比色皿,中心高度应该怎么选? 已有2人参与

请教各位:谱析TU-1810和PE Lambda 25紫外可见光谱仪,想配50微升比色皿,中心高度的规格有8,15,20mm,请问应该选多少mm?非常感谢! @学术巨星
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wenlingd

至尊木虫 (著名写手)

【答案】应助回帖

感谢参与,应助指数 +1
这个问厂家,他们一定会提供解决方案的

[ 发自手机版 http://muchong.com/3g ]
2楼2019-04-13 05:45:24
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sunnyyang09

捐助贵宾 (小有名气)

引用回帖:
2楼: Originally posted by wenlingd at 2019-04-13 05:45:24
这个问厂家,他们一定会提供解决方案的

非常感谢您的回复!
3楼2019-04-15 13:39:58
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hxy211422

银虫 (小有名气)

【答案】应助回帖

不同厂家中心高度:https://www.starna.com/starna-cells/cell-height-finder
自己检测中心高度的方法:https://www.starna.com/cells/z-dimension

How can I determine the Z Dimension of my instrument myself?

Some instruments have cell holders with different z heights, or where the z height can be varied in respect to the alignment with the instrument light beam. It is therefore useful to know how to determine the z height oneself.

Method 1

You can test for the Z dimension of your instrument yourself very easily. Simply follow these steps:
1) Cut a piece of dense white card or paper 12 mm wide and 100 mm long (approximately).
2) Make a hole in the centre of the paper about 3 mm in diameter (just push a ballpoint pen through the paper) 8.5 mm from the bottom of one end and 15 mm from the bottom of the other.
3) Turn on your spectrophotometer in %T mode and set to any reasonable wavelength.
4) Place the piece of paper with the hole in the end into the cell holder as if it were a cell. Whichever end (either 8.5mm or 15mm) transmits light will tell you the Z dimension of your instrument.
5) If neither works then make up another piece of paper with holes placed at different dimensions and determine which works best.

Method 2

Alternatively if you can easily access the sample compartment, a simple method to determine this height would be to set the instrument to measure at a visible wavelength (546 nm for example), insert a piece of white card into the sample compartment and then mark the card with a pen/pencil where the beam intersects. The distance from the bottom of the card to the mark should give the approximate height of the beam.
4楼2019-04-23 10:11:22
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