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shenjianxiandao木虫 (正式写手)
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[交流]
求助一无机物的红外谱图分析
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最近，我用SiO2（自制，未洗净含有NaCl）负载质量分数5%硫酸盐作为催化剂，在500度时焙烧后并在500度反应，反应后催化剂表面有积碳，可能有—O—Sx+，或—O—Sx-，或—S—Sx+，或—S—Sx-，或金属离子与S形成的配位键（个人认为可能性比较小），未验证上诉可能情况，做了一下红外，谱图如下，请达人帮忙分析 [ Last edited by shenjianxiandao on 2009-5-3 at 17:06 ] |
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铁杆木虫 (职业作家)
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9楼2009-05-04 12:02:51
shenjianxiandao
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红外数据如下 399.1992 0.15307 401.1277 0.16629 403.0562 0.17269 404.9847 0.17488 406.9132 0.17627 408.8417 0.18009 410.7702 0.18239 412.6987 0.18691 414.6272 0.19352 416.5557 0.19996 418.4842 0.20738 420.4127 0.2199 422.3412 0.2274 424.2697 0.2351 426.1982 0.24191 428.1267 0.24845 430.0552 0.25397 431.9837 0.26166 433.9122 0.27163 435.8407 0.28494 437.7692 0.29957 439.6977 0.31291 441.6262 0.32708 443.5547 0.34472 445.4832 0.35901 447.4117 0.36767 449.3401 0.3735 451.2686 0.3804 453.1971 0.39092 455.1256 0.40335 457.0541 0.42056 458.9826 0.44563 460.9111 0.4672 462.8396 0.49223 464.7681 0.51947 466.6966 0.54712 468.6251 0.57657 470.5536 0.60272 472.4821 0.62219 474.4106 0.63695 476.3391 0.647 478.2676 0.65701 480.1961 0.66359 482.1246 0.66982 484.0531 0.67603 485.9816 0.67737 487.9101 0.66916 489.8386 0.65368 491.7671 0.63297 493.6956 0.6148 495.6241 0.60033 497.5526 0.58736 499.4811 0.57647 501.4096 0.56678 503.3381 0.55608 505.2666 0.54638 507.1951 0.53731 509.1236 0.52837 511.0521 0.51873 512.9806 0.50788 514.9091 0.49449 516.8376 0.47818 518.7661 0.45766 520.6946 0.43526 522.6231 0.41106 524.5516 0.38604 526.4801 0.35879 528.4086 0.332 530.3371 0.30589 532.2656 0.28398 534.1941 0.26698 536.1226 0.25247 538.0511 0.23733 539.9796 0.22149 541.9081 0.20516 543.8365 0.19029 545.7651 0.1777 547.6935 0.16913 549.6221 0.16299 551.5505 0.15736 553.4791 0.15099 555.4075 0.14389 557.3361 0.13517 559.2645 0.12672 561.1931 0.11982 563.1215 0.11527 565.05 0.11262 566.9786 0.11165 568.907 0.11008 570.8356 0.10756 572.764 0.10312 574.6926 0.0971 576.621 0.09036 578.5496 0.08524 580.478 0.08155 582.4066 0.08019 584.335 0.08015 586.2635 0.08034 588.192 0.07951 590.1205 0.07737 592.049 0.07287 593.9775 0.0679 595.906 0.06357 597.8345 0.06145 599.763 0.06166 601.6915 0.06424 603.62 0.06787 605.5485 0.07211 607.477 0.07626 609.4055 0.08126 611.334 0.08873 613.2625 0.10169 615.191 0.11954 617.1195 0.13886 619.048 0.15324 620.9765 0.15977 622.905 0.15904 624.8335 0.1529 626.762 0.14143 628.6905 0.12721 630.619 0.11201 632.5475 0.09868 634.476 0.08814 636.4045 0.08086 638.333 0.07643 640.2615 0.07395 642.19 0.07105 644.1185 0.06748 646.047 0.06244 647.9755 0.0563 649.904 0.04961 651.8325 0.04451 653.761 0.0415 655.6895 0.04071 657.618 0.041 659.5464 0.04181 661.475 0.04148 663.4034 0.03962 665.332 0.03635 667.2604 0.0328 669.189 0.02753 671.1174 0.02495 673.046 0.02434 674.9745 0.02546 676.903 0.0269 678.8315 0.02814 680.7599 0.02773 682.6885 0.02546 684.6169 0.02159 686.5455 0.01761 688.4739 0.01458 690.4025 0.01357 692.3309 0.01422 694.2595 0.01608 696.1879 0.01783 698.1165 0.01873 700.0449 0.01763 701.9734 0.01502 703.9019 0.01144 705.8304 0.00843 707.7589 0.00671 709.6874 0.00706 711.6159 0.00877 713.5444 0.01111 715.4729 0.013 717.4014 0.0138 719.3299 0.01267 721.2584 0.01022 723.1869 0.00734 725.1154 0.00579 727.0439 0.00597 728.9724 0.00802 730.9009 0.01098 732.8294 0.01418 734.7579 0.01623 736.6864 0.01693 738.6149 0.01615 740.5434 0.01487 742.4719 0.01371 744.4004 0.0141 746.3289 0.01629 748.2574 0.01997 750.1859 0.02428 752.1144 0.02849 754.0429 0.03167 755.9714 0.03407 757.8999 0.03575 759.8284 0.03775 761.7569 0.04103 763.6854 0.04691 765.6139 0.05572 767.5424 0.0673 769.4709 0.08117 771.3994 0.09715 773.3279 0.11501 775.2563 0.13412 777.1849 0.15397 779.1133 0.17386 781.0419 0.19363 782.9703 0.21355 784.8989 0.23425 786.8274 0.25457 788.7559 0.27307 790.6844 0.28738 792.6129 0.29577 794.5414 0.29638 796.4698 0.29009 798.3984 0.2765 800.3268 0.25671 802.2554 0.23237 804.1838 0.20696 806.1124 0.18248 808.0408 0.16039 809.9694 0.1407 811.8978 0.12327 813.8264 0.10774 815.7548 0.09385 817.6833 0.082 819.6118 0.0724 821.5403 0.06512 823.4688 0.05959 825.3973 0.05537 827.3258 0.05124 829.2543 0.04679 831.1828 0.0416 833.1113 0.03601 835.0398 0.03034 836.9683 0.02574 838.8969 0.02252 840.8253 0.02072 842.7538 0.01957 844.6823 0.01881 846.6108 0.01748 848.5393 0.01538 850.4678 0.01236 852.3963 0.00919 854.3248 0.0063 856.2533 0.00457 858.1818 0.00383 860.1103 0.00415 862.0388 0.00465 863.9673 0.00507 865.8958 0.00474 867.8243 0.00377 869.7528 0.0022 871.6813 7.98255E-4 873.6098 0 875.5383 3.90753E-4 877.4668 0.00152 879.3953 0.00332 881.3238 0.00502 883.2523 0.0065 885.1808 0.0073 887.1093 0.00754 889.0378 0.00743 890.9662 0.00795 892.8948 0.00917 894.8233 0.01141 896.7518 0.01429 898.6803 0.01748 900.6088 0.02033 902.5373 0.02276 904.4658 0.02456 906.3943 0.02616 908.3228 0.02771 910.2513 0.02994 912.1797 0.03293 914.1083 0.0367 916.0367 0.04076 917.9653 0.04491 919.8937 0.04851 921.8223 0.05174 923.7507 0.05448 925.6793 0.05713 927.6077 0.06006 929.5363 0.06369 931.4647 0.06791 933.3932 0.0727 935.3217 0.07767 937.2502 0.08247 939.1787 0.08661 941.1072 0.09032 943.0357 0.09384 944.9642 0.09748 946.8927 0.10146 948.8212 0.10608 950.7498 0.11129 952.6782 0.1168 954.6068 0.12213 956.5352 0.12701 958.4637 0.1315 960.3922 0.13562 962.3207 0.1396 964.2492 0.14389 966.1777 0.14876 968.1062 0.15417 970.0347 0.15998 971.9632 0.1659 973.8917 0.17171 975.8202 0.17707 977.7487 0.18205 979.6772 0.18689 981.6057 0.19206 983.5342 0.19774 985.4627 0.20424 987.3912 0.21146 989.3197 0.21905 991.2482 0.22595 993.1767 0.23194 995.1052 0.2369 997.0337 0.24184 998.9622 0.24708 1000.891 0.25312 1002.819 0.2597 1004.748 0.267 1006.676 0.27465 1008.605 0.28277 1010.533 0.29051 1012.462 0.29807 1014.39 0.3052 1016.319 0.31254 1018.247 0.31985 1020.176 0.32779 1022.104 0.33601 1024.033 0.34507 1025.961 0.35419 1027.89 0.36382 1029.818 0.37305 1031.747 0.38241 1033.675 0.39123 1035.604 0.40052 1037.532 0.4097 1039.461 0.41995 1041.389 0.43042 1043.318 0.4419 1045.246 0.45337 1047.175 0.46568 1049.103 0.4776 1051.032 0.49028 1052.96 0.5027 1054.889 0.51688 1056.817 0.53192 1058.746 0.54973 1060.674 0.56882 1062.603 0.59103 1064.531 0.61456 1066.46 0.64121 1068.388 0.66923 1070.317 0.70109 1072.245 0.73289 1074.174 0.76549 1076.102 0.79555 1078.031 0.82873 1079.959 0.8617 1081.888 0.89743 1083.816 0.93014 1085.745 0.96532 1087.673 0.99687 1089.602 1.02949 1091.53 1.05487 1093.459 1.07996 1095.387 1.09721 1097.316 1.1136 1099.244 1.11801 1101.173 1.11989 1103.101 1.11185 1105.03 1.10319 1106.958 1.08723 1108.887 1.07338 1110.815 1.05376 1112.744 1.03759 1114.672 1.01821 1116.601 1.00256 1118.529 0.98468 1120.458 0.97122 1122.386 0.95528 1124.315 0.94364 1126.243 0.9296 1128.172 0.91877 1130.1 0.90573 1132.029 0.8958 1133.957 0.88362 1135.886 0.87423 1137.814 0.86323 1139.743 0.85556 1141.671 0.84582 1143.6 0.83844 1145.528 0.82898 1147.457 0.82135 1149.385 0.8111 1151.314 0.80246 1153.242 0.79144 1155.171 0.78224 1157.099 0.77095 1159.028 0.76137 1160.956 0.74957 1162.885 0.7391 1164.813 0.72665 1166.742 0.71528 1168.67 0.70126 1170.599 0.68805 1172.527 0.67272 1174.456 0.65826 1176.384 0.64198 1178.313 0.62672 1180.241 0.61001 1182.17 0.59467 1184.098 0.5789 1186.026 0.56538 1187.955 0.55314 1189.884 0.54556 1191.812 0.54186 1193.74 0.54387 1195.669 0.54766 1197.598 0.55189 1199.526 0.55235 1201.454 0.55028 1203.383 0.54387 1205.312 0.53617 1207.24 0.52601 1209.168 0.51614 1211.097 0.50553 1213.026 0.4956 1214.954 0.48467 1216.882 0.47453 1218.811 0.46337 1220.74 0.45278 1222.668 0.44142 1224.597 0.43084 1226.525 0.4198 1228.453 0.40995 1230.382 0.40024 1232.311 0.39203 1234.239 0.38412 1236.167 0.3775 1238.096 0.37079 1240.025 0.36473 1241.953 0.35814 1243.881 0.35187 1245.81 0.3449 1247.739 0.33851 1249.667 0.33215 1251.595 0.32654 1253.524 0.32084 1255.453 0.31577 1257.381 0.31015 1259.309 0.30464 1261.238 0.29839 1263.167 0.29225 1265.095 0.28577 1267.023 0.2799 1268.952 0.27426 1270.88 0.26964 1272.809 0.26528 1274.737 0.26162 1276.666 0.2577 1278.594 0.25384 1280.523 0.24938 1282.451 0.24495 1284.38 0.24045 1286.308 0.23659 1288.237 0.23307 1290.165 0.23052 1292.094 0.22811 1294.022 0.22603 1295.951 0.22352 1297.879 0.22086 1299.808 0.2176 1301.736 0.21437 1303.665 0.21114 1305.593 0.20858 1307.522 0.20643 1309.45 0.20499 1311.379 0.2036 1313.307 0.20234 1315.236 0.20055 1317.164 0.19845 1319.093 0.1957 1321.021 0.19314 1322.95 0.19074 1324.878 0.18892 1326.807 0.18739 1328.735 0.18652 1330.664 0.18571 1332.592 0.18477 1334.521 0.18313 1336.449 0.18106 1338.378 0.17841 1340.306 0.17605 1342.235 0.17427 1344.163 0.17302 1346.092 0.17203 1348.02 0.17155 1349.949 0.17093 1351.877 0.17023 1353.806 0.16873 1355.734 0.16686 1357.663 0.16472 1359.591 0.16272 1361.52 0.16072 1363.448 0.15966 1365.377 0.15939 1367.305 0.15921 1369.234 0.15875 1371.162 0.15815 1373.091 0.15656 1375.019 0.15479 1376.948 0.15331 1378.876 0.15202 1380.805 0.15129 1382.733 0.1516 1384.662 0.15173 1386.59 0.1509 1388.519 0.1496 1390.447 0.14862 1392.376 0.14707 1394.304 0.145 1396.233 0.14294 1398.161 0.14169 1400.09 0.14081 1402.018 0.14071 1403.947 0.14045 1405.875 0.14047 1407.804 0.14022 1409.732 0.13948 1411.661 0.1381 1413.589 0.13658 1415.518 0.1348 1417.446 0.13324 1419.375 0.13223 1421.303 0.13238 1423.232 0.13233 1425.16 0.13253 1427.089 0.13232 1429.017 0.13145 1430.946 0.13004 1432.874 0.12871 1434.803 0.12729 1436.731 0.12607 1438.66 0.12571 1440.588 0.12587 1442.517 0.12594 1444.445 0.12596 1446.374 0.12537 1448.302 0.12435 1450.231 0.12316 1452.159 0.12182 1454.088 0.12034 1456.016 0.11896 1457.945 0.11826 1459.873 0.11907 1461.802 0.11954 1463.73 0.1193 1465.659 0.11856 1467.587 0.11785 1469.516 0.11645 1471.444 0.11451 1473.373 0.11263 1475.301 0.11215 1477.23 0.11211 1479.158 0.11234 1481.087 0.11224 1483.015 0.11209 1484.944 0.11133 1486.872 0.10998 1488.801 0.10823 1490.729 0.10704 1492.658 0.10666 1494.586 0.10627 1496.515 0.10575 1498.443 0.10599 |
2楼2009-05-03 10:21:29
shenjianxiandao
木虫 (正式写手)
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1500.372 0.1063 1502.3 0.10624 1504.229 0.10547 1506.157 0.10331 1508.086 0.1014 1510.014 0.10166 1511.943 0.10144 1513.871 0.10112 1515.8 0.10055 1517.728 0.10077 1519.657 0.10077 1521.585 0.10005 1523.514 0.09961 1525.442 0.09886 1527.371 0.09792 1529.299 0.09745 1531.228 0.09683 1533.156 0.09632 1535.085 0.09683 1537.013 0.09696 1538.942 0.09596 1540.87 0.09494 1542.799 0.09462 1544.727 0.09412 1546.656 0.09362 1548.584 0.09293 1550.513 0.09234 1552.441 0.09237 1554.37 0.09224 1556.298 0.09202 1558.227 0.09072 1560.155 0.09086 1562.084 0.09116 1564.012 0.09049 1565.941 0.08961 1567.869 0.08893 1569.798 0.08856 1571.726 0.08929 1573.655 0.08953 1575.583 0.08939 1577.512 0.0896 1579.44 0.08974 1581.369 0.0893 1583.297 0.0887 1585.226 0.08824 1587.154 0.08825 1589.083 0.08854 1591.011 0.0892 1592.94 0.08988 1594.868 0.09046 1596.797 0.0909 1598.725 0.09104 1600.654 0.09076 1602.582 0.09055 1604.511 0.09065 1606.439 0.09106 1608.368 0.09174 1610.296 0.09285 1612.225 0.09388 1614.153 0.0944 1616.082 0.09438 1618.01 0.09466 1619.939 0.09471 1621.867 0.09427 1623.796 0.09415 1625.724 0.09458 1627.653 0.09489 1629.581 0.09553 1631.51 0.09567 1633.438 0.09516 1635.367 0.09362 1637.295 0.0927 1639.224 0.09226 1641.152 0.09146 1643.081 0.09053 1645.009 0.08955 1646.938 0.08832 1648.866 0.08853 1650.795 0.08833 1652.723 0.08689 1654.652 0.08551 1656.58 0.08526 1658.509 0.08424 1660.437 0.08293 1662.366 0.08159 1664.294 0.08119 1666.223 0.0809 1668.151 0.08009 1670.08 0.07915 1672.008 0.07871 1673.937 0.07775 1675.865 0.07634 1677.794 0.07522 1679.722 0.07407 1681.651 0.07301 1683.579 0.07201 1685.508 0.07212 1687.436 0.07242 1689.365 0.07207 1691.293 0.07167 1693.222 0.07078 1695.15 0.06924 1697.079 0.0676 1699.007 0.06711 1700.936 0.06681 1702.864 0.06699 1704.793 0.06687 1706.721 0.06716 1708.65 0.06733 1710.578 0.06695 1712.507 0.06614 1714.435 0.06489 1716.364 0.06382 1718.292 0.06376 1720.221 0.06441 1722.149 0.06476 1724.078 0.06508 1726.006 0.06541 1727.935 0.06516 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3楼2009-05-03 10:23:19
shenjianxiandao
木虫 (正式写手)
- 应助: 3 (幼儿园)
- 金币: 4203.3
- 散金: 6
- 红花: 1
- 帖子: 433
- 在线: 125.7小时
- 虫号: 450470
- 注册: 2007-11-04
- 性别: GG
- 专业: 化学反应工程
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3629.434 0.01077 3631.363 0.01058 3633.291 0.01039 3635.219 0.01021 3637.148 0.01007 3639.076 0.00982 3641.005 0.00959 3642.934 0.0092 3644.862 0.00871 3646.791 0.00811 3648.719 0.00736 3650.647 0.00707 3652.576 0.00743 3654.504 0.00763 3656.433 0.00732 3658.362 0.00707 3660.29 0.00699 3662.219 0.00696 3664.147 0.00683 3666.075 0.00659 3668.004 0.00625 3669.932 0.00592 3671.861 0.00587 3673.79 0.00578 3675.718 0.00525 3677.646 0.00538 3679.575 0.00556 3681.503 0.00549 3683.432 0.00532 3685.36 0.00503 3687.289 0.00453 3689.218 0.00405 3691.146 0.0044 3693.074 0.00474 3695.003 0.00478 3696.931 0.00474 3698.86 0.00461 3700.788 0.00432 3702.717 0.00406 3704.646 0.00411 3706.574 0.00408 3708.502 0.00401 3710.431 0.00381 3712.359 0.00374 3714.288 0.00381 3716.216 0.00395 3718.145 0.00389 3720.073 0.00376 3722.002 0.00368 3723.93 0.00374 3725.859 0.00384 3727.787 0.004 3729.716 0.00408 3731.644 0.00384 3733.573 0.0033 3735.501 0.00305 3737.43 0.00313 3739.358 0.00344 3741.287 0.00361 3743.215 0.00401 3745.144 0.00373 3747.073 0.00321 3749.001 0.00326 3750.929 0.00314 3752.858 0.00318 3754.786 0.00332 3756.715 0.00334 3758.643 0.00325 3760.572 0.00336 3762.5 0.00341 3764.429 0.00341 3766.357 0.00335 3768.286 0.00346 3770.214 0.00345 3772.143 0.00351 3774.071 0.00359 3776 0.00351 3777.928 0.00328 3779.857 0.00317 3781.785 0.0034 3783.714 0.00351 3785.642 0.00348 3787.571 0.00368 3789.499 0.00375 3791.428 0.00374 3793.356 0.00361 3795.285 0.00335 3797.213 0.00316 3799.142 0.00319 3801.07 0.00323 3802.999 0.0032 3804.927 0.00347 3806.856 0.00365 3808.784 0.00368 3810.713 0.00379 3812.641 0.0037 3814.57 0.00364 3816.498 0.00349 3818.427 0.00334 3820.355 0.00345 3822.284 0.0036 3824.212 0.00372 3826.141 0.00374 3828.069 0.00387 3829.998 0.00401 3831.926 0.0039 3833.855 0.00374 3835.783 0.00344 3837.712 0.00337 3839.64 0.00341 3841.569 0.00374 3843.497 0.00394 3845.426 0.00403 3847.354 0.0041 3849.283 0.00394 3851.211 0.00378 3853.14 0.00396 3855.068 0.0039 3856.997 0.00393 3858.925 0.00427 3860.854 0.00435 3862.782 0.00416 3864.711 0.00409 3866.639 0.00416 3868.568 0.00441 3870.496 0.00419 3872.425 0.00414 3874.353 0.00434 3876.282 0.00457 3878.21 0.00452 3880.139 0.00434 3882.067 0.00439 3883.996 0.0044 3885.924 0.00442 3887.853 0.00463 3889.781 0.0047 3891.71 0.00461 3893.638 0.00481 3895.567 0.00494 3897.495 0.00483 3899.424 0.00467 3901.352 0.00464 3903.281 0.00462 3905.209 0.00465 3907.138 0.00494 3909.066 0.0052 3910.995 0.00526 3912.923 0.00521 3914.852 0.00524 3916.78 0.00517 3918.709 0.00519 3920.637 0.00533 3922.566 0.00538 3924.494 0.00527 3926.423 0.00535 3928.351 0.00532 3930.28 0.00517 3932.208 0.00524 3934.137 0.00542 3936.065 0.00567 3937.994 0.00578 3939.922 0.0058 3941.851 0.00564 3943.779 0.0055 3945.708 0.00562 3947.636 0.00563 3949.565 0.00559 3951.493 0.00574 3953.422 0.00599 3955.35 0.00611 3957.279 0.00609 3959.207 0.00613 3961.136 0.00615 3963.064 0.00615 3964.993 0.00615 3966.921 0.00616 3968.85 0.00618 3970.778 0.00625 3972.707 0.00628 3974.635 0.00633 |
4楼2009-05-03 10:23:53