| 查看: 7164 | 回复: 21 | |||
| 当前主题已经存档。 | |||
| 当前只显示满足指定条件的回帖，点击这里查看本话题的所有回帖 | |||
[交流]
【求助】玻璃的硅烷化处理
|
|||
| 看了一篇文献，发现需要玻璃的硅烷化处理，有做过的同学吗，请教一下，需要什么样的试剂，及如何处理，谢谢！ |
回复此楼
乃容斋
木虫 (正式写手)
- 应助: 2 (幼儿园)
- 金币: 2466.8
- 散金: 102
- 红花: 1
- 帖子: 760
- 在线: 355.3小时
- 虫号: 485995
- 注册: 2007-12-27
- 性别: GG
- 专业: 电机与电器
★ ★ ★
小木虫(金币+0.5):给个红包，谢谢回帖交流
jason168(金币+2,VIP+0):欢迎交流！ 6-2 20:30
小木虫: 金币+2, 帖子真精彩 2014-09-18 10:59:47
小木虫(金币+0.5):给个红包，谢谢回帖交流
jason168(金币+2,VIP+0):欢迎交流！ 6-2 20:30
小木虫: 金币+2, 帖子真精彩 2014-09-18 10:59:47
|
我最近也在了解这方面的问题，我做的是纳米线不过。下面是我做的一个方法的总结，不知道对你有没有帮助。 1）氧等离子体处理（清洗和产生羟基）或清洗后The NWs devices were then placed in the ozone/UV chamber for 3 minutes. 2) piranha solution（浓硫酸和30%双氧水 v/v3:1）浸泡5 min, 分别在 H2O 和acetone 超声20 min， 再用 5 M NaOH 室温处理5min ,水清洗，1% APTMS 水或醇溶液处理 10-15 min硅烷化修饰。 3）hydroxylated using a NaOH solution (4M in ethanol 95%) during 2 h.This treatment creates OH groups and eliminates organic contamination. The samples are placed for 12 h in a solution 0.5M of APTES in 95% ethanol. After two successive rinses with ethanol and deionised water to remove unbound silane,the samples are dried and heated for 3 h at 110 ◦C. 4）the SnO2 films were immersed in 1% ethanol solution of APTES for 3 min at room temperature,rinsed with ethanol for three times, then heated at 125 ◦C for 15 min 5) First, the samples were sonicated in 0.2%(v/v) soapy water at 60 ℃, thoroughly washed with triple distilled water (TDW), and then dipped in hot (90 ℃) piranha solution for 60 min (3:7 by volume of 30% H2O2 :H2SO4 Afterward, substrates were rinsed with TDW and further cleaned with H2O/H2O2/NH3 (5:1:0.25) solution while sonicating for 15 min at 60 ℃. |
14楼2009-06-02 20:11:36
yccycc
木虫 (著名写手)
- 应助: 17 (小学生)
- 金币: 1921.7
- 散金: 10
- 红花: 4
- 帖子: 1076
- 在线: 64.2小时
- 虫号: 478326
- 注册: 2007-12-14
- 专业: 无机非金属类光电信息与功
2楼2009-04-28 07:31:45
3楼2009-04-28 13:28:02
gywu0420
铁杆木虫 (知名作家)
- 应助: 1 (幼儿园)
- 金币: 9236.4
- 沙发: 2
- 帖子: 9859
- 在线: 403.5小时
- 虫号: 669608
- 注册: 2008-12-07
- 性别: GG
- 专业: 无机非金属基复合材料
4楼2009-04-28 15:36:58