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Scanning Electrochemical Microscopy
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Scanning Electrochemical Microscopy Ed. Allen J. Bard, Michael V. Mirkin Publisher: Marcel Dekker | ISBN: 0824704711 | 2001 | Pages: 664 | PDF  This reference describes the theory and operating principles of scanning electrochemical microscopy (SECM), including instrumentation, tip preparation, imaging techniques, and potentiometric probes, and explores applications to electron transfer reactions, reaction kinetics, chemical events at interfaces, biological systems, and fabrication. Table of Contents Preface iii Contributors ix 1 Introduction and Principles 1 I. Background of Scanning Electrochemical Microscopy 1 II. Principles of SECM 2 III. Applications of SECM 9 References 15 2 Instrumentation 17 I. Introduction 17 II. Overview of the SECM Apparatus 18 III. Commercial SECM Instrument Implementation 42 IV. Tip Position Modulation Instrumentation 44 V. Constant-Current Mode Instrumentation 44 VI. Experimental Difficulties in Data Acquisition 53 VII. Accessory Equipment for SECM 59 Appendix; Suppliers 66 References 71 3 The Preparation of Tips for Scanning Electrochemical Microscopy 75 I. Introduction 75 II. Preparation Techniques 75 III. Nondisk Tips and Tip Shape Characterization 104 References 107 4 Secm Imaging 111 I. Introduction 111 II. Principle and Methodology of SEM Imaging 111 III. Images in Solutions 115 IV. Images in Humid Air 124 V. Conclusions and Future Projections 139 References 141 5 Theory 145 I. Introduction 145 II. Feedback Mode of SECM Operation 145 III. Generation/Collection (G/C) Mode of SECM Operation 165 IV. SECM of More Complicated Chemical Systems 170 V. Numerical Solution of SECM Diffusion Problems Using PDEase 2 Program Package 182 List of Symbols 193 References 198 6 Heterogeneous Electron Transfer Reactions 201 I. Introduction 201 II. Principles 203 III. Studies of Heterogeneous Electron Transfer 217 IV. Applications 234 V. Conclusion and Outlook 237 References 238 7 Kinetics of Homogeneous Reactions Coupled to Heterogeneous Electron Transfer 241 I. Introduction 241 II. EC[subscript i] Processes 244 III. EC[subscript 2i] Processes 270 IV. ECE/DISP Processes 283 References 297 8 Charge-Transfer at the Liquid/Liquid Interface 299 I. Introduction 299 II. Electron Transfer 301 III. Ion Transfer at the ITIES 325 IV. Processes with Coupled Homogeneous Reactions 336 References 339 9 Imaging Molecular Transport Across Membranes 343 I. Introduction 343 II. Principles of Imaging Porous Membranes 346 III. Applications 365 IV. Future Directions 392 References 394 10 Potentiometric Probes 397 I. Introduction 397 II. Basic Theory 415 III. Properties and Behavior of Ion-Selective Probes 417 IV. Potentiometric Measurements in Scanning Probe Microscopies Other than SECM 422 V. Potentiometric Measurements in SECM 423 VI. Conclusion 441 References 442 11 Biological Systems 445 I. Approaches to Imaging Biological and Biochemical Systems 445 II. Selected Applications 463 III. Conclusion and Outlook 504 IV. Abbreviations, Acronyms, and Symbols 510 References 512 12 Probing Reactions at Solid/Liquid Interfaces 521 I. Introduction 521 II. Measurement of Adsorption/Desorption Kinetics and Surface Diffusion Rates 523 III. Dissolution Kinetics of Ionic Single Crystals 536 IV. Corrosion Studies 573 V. Conclusions 588 References 590 13 Micro- and Nanopatterning Using the Scanning Electrochemical Microscope 593 I. Patterning by the Direct Mode of the SECM 594 II. Patterning by the Feedback Mode of the SECM 603 III. Perspective Approaches 623 References 625 14 Conclusions and Prospects 629 I. Combining SECM with Other Techniques 629 II. Novel Interfaces 634 III. Instrumentation Improvements 636 References 637 Index 639 http://www.namipan.com/d/ScanElectrochemicalMicro.pdf/4cc6b33eefb1cf37ea1061f8df50d0b3eee330375f2a8c00 [ Last edited by yensh on 2009-6-18 at 18:42 ] |
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