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wupeng087916

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[交流] 水热法制备TiO2纳米线

有谁用这篇文献的方法制备出TiO2纳米线的?
文献“Hydrothermal synthesis and photoluminescence of TiO2 nanowires”

In a typical preparation procedure, 1 g anatase TiO2 white powders were placed
into a Teflon-lined autoclave of 50 ml capacity.
Then, the autoclave was filled with 10 M NaOH
aqueous solution up to 80% of the total volume,
sealed into a stainless steel tank and maintained at
200 C for 24 h without shaking or stirring during
the heating. After the autoclave was naturally
cooled to room temperature, the obtained sample
was sequentially washed with dilute HCl aqueous
solution, distilled deionized water and absolute
ethanol for several times. The samples were dried
at 70 C for 6 h. Finally, soft fibrous powders with
white color were obtained.
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wupeng087916(金币+1): 谢谢参与
2楼2017-11-02 21:26:46
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3楼2017-11-02 22:03:51
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4楼2017-11-02 22:16:32
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