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lattice parameters for Co2C and MnO were perdetermined in a separate refinement for the 150-hour sample and kept fixed during the refinements. For akk specimens, the scale factors, profile shape and broadening parameters, asymmetry and correction for preferred orientation were refined during the quantitative analysis ¸Õ¿ªÊ¼¿´Ó¢ÎÄÎÄÏ×£¬ Ï£ÍûÄÜУÕýÏ ӢÎĵÄÊõÓï лл |
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