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[交流]
磁性介孔硅的氮吸附脱附和孔径分布图怎么做，求大神指教
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| 第一次做氮吸咐脱附，老师直接给的数据，是不是有问题啊，很多数据都不清楚，请大家指教下，是不是数据有问题啊 |
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erdange: 金币+5 2017-03-21 20:45:34
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erdange: 金币+5 2017-03-21 20:45:34
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2楼2017-03-20 18:04:50
17864279858
铜虫 (初入文坛)
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3楼2017-03-21 14:52:21
4楼2017-03-21 20:40:03
5楼2017-03-21 20:44:02
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不好意思啊，我不太熟练呢。 Quantachrome QuadraWin - Data Acquisition and Reduction for QuadraSorb SI ?2000-13, Quantachrome Instruments. All rights reserved. version 6.0 Analysis Report Operator: operator Date:3/1/2017 Operator: operator Date:2017/03/02 Sample ID: 介孔 Filename: QW1_170301_01样品1.QPS Sample Desc: Comment: Sample weight: 0.4711 g Analysis Time: 554.5 min End of run: 3/1/2017 18:32:34 Instrument: QuadraSorb Station 1 Void Vol.: He Mode.Cell: 9mm large bulbRun mode:Standard Instrument version:6.00 Cold Zone Vol.:29.1045 Warm Zone Vol.:13.1646 Thermal delay: 30 sec He evac time: 3 min Outgas Time: 3.0 hrs OutgasTemp: 300.0 C Analysis gas: Nitrogen Bath Temp: 77.3 K Press. Tolerance:0.050/0.050 (ads/des)Equil time: 60/60 sec (ads/des) Equil timeout: 240/240 sec (ads/des) Press P0 Volume @ STP Tol TimeOut EquLibration Torr Torr cc sec 38.25 777.29 11.5053 0.05 240 60 77.08 777.27 13.2513 0.05 240 60 115.81 776.45 14.4828 0.05 240 60 155.16 776.69 15.5222 0.05 240 60 193.81 777.00 16.4331 0.05 240 60 233.01 776.45 17.2472 0.05 240 60 272.01 776.87 18.0639 0.05 240 60 |
6楼2017-03-21 20:44:49
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Quantachrome QuadraWin - Data Acquisition and Reduction for QuadraSorb SI ?2000-13, Quantachrome Instruments. All rights reserved. version 6.0 Analysis Report Operator: operator Date:3/1/2017 Operator: operator Date:2017/03/02 Sample ID: 介孔 Filename: QW1_170301_01样品1.QPS Sample Desc: Comment: Sample weight: 0.4711 g Analysis Time: 554.5 min End of run: 3/1/2017 18:32:34 Instrument: QuadraSorb Station 1 Void Vol.: He Mode.Cell: 9mm large bulbRun mode:Standard Instrument version:6.00 Cold Zone Vol.:29.1045 Warm Zone Vol.:13.1646 Thermal delay: 30 sec He evac time: 3 min Outgas Time: 3.0 hrs OutgasTemp: 300.0 C Analysis gas: Nitrogen Bath Temp: 77.3 K Press. Tolerance:0.050/0.050 (ads/des)Equil time: 60/60 sec (ads/des) Equil timeout: 240/240 sec (ads/des) Data Reduction Parameters Adsorbate Nitrogen Temperature 77.350K Molec. Wt.: 28.013 Cross Section: 16.200 舿2 Liquid Density: 0.808 g/cc Relative Volume @ STP 1 / [ W((Po/P) - 1) ] Pressure P/Po cc/g 4.92047e-02 24.4223 1.6954e+00 9.91724e-02 28.1284 3.1315e+00 1.49157e-01 30.7426 4.5625e+00 1.99765e-01 32.9489 6.0619e+00 2.49429e-01 34.8823 7.6225e+00 3.00095e-01 36.6105 9.3705e+00 BET summary Slope = 30.385 Intercept = 1.062e-01 Correlation coefficient, r = 0.999349 C constant= 287.126 Surface Area = 114.215 m?g |
7楼2017-03-21 20:47:48
8楼2017-03-21 20:47:57
17864279858
铜虫 (初入文坛)
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9楼2017-03-30 09:13:44
