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Herein, we introduce a simple and scalable top-down strategy for the phase- and morphology-controlled synthesis of FePO4·2H2O via the phosphation of β-FeOOH nanorods (nr), synthesised via hydrothermal hydrolysis of FeCl3 (Fig. 1). Subsequent annealing of the hydrated iron phos?phates leads to different polymorphs of FePO4. An array of characterisation techniques are employed to unravel the ki?netics and mechanism of the crystallisation of FePO4·2H2O in different phases. 发自小木虫Android客户端 |
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