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Diffraction data for all of the donors were collected with Mo-Ka radiation (l= 0.71070 ? on a Bruker AXS APEX II CCD diffractome?ter equipped with a Japan Thermal Engineering Cryosystem DX?CS10KLD. All the structures were solved by a direct method using SHELXS-97 [13] and refined by the full-matrix least squares technique. Absorption corrections were applied using the multi?scan procedure with SADABS. All non-hydrogen atoms were refined anisotropically for all the structures. The positions of hydrogen atoms were calculated with sp2 or sp3 configurations of the bonding carbon atoms and included in the analysis. 发自小木虫Android客户端 |
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