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To measure overpotential dependence, lithium half-cells were potentiostatically and galvanostatically cycled while diffraction data were obtained in situ. These tests were performed on two reference (undoped) Li1-xFePO4 powders for which extensive data have previously been obtained.3,9-11 The starting powders were prepared as composite electrode coatings on aluminum foil current collectors and assembled in modified lithium half-cells. Powder diffraction spectra were collected in transmission mode using a linear position-sensitive silicon detector 发自小木虫Android客户端 |
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