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Environmental Laboratory Exercises for Instrumental Analysis
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Environmental Laboratory Exercises for Instrumental Analysis and Environmental Chemistry Frank M. Dunnivant ISBN: 978-0-471-48856-9 Paperback 416 pages August 2004 Wiley List Price: US $95.50 A comprehensive set of real-world environmental laboratory experimentsThis complete summary of laboratory work presents a richly detailed setof classroom-tested experiments along with background information,safety and hazard notes, a list of chemicals and solutions needed, datacollection sheets, and blank pages for compiling results and findings.This useful resource also: Focuses on environmental, i.e., "dirty" samples Stresses critical concepts like analysis techniques and documentation Includes water, air, and sediment experiments Includes an interactive software package for pollutant fate and transport modeling exercises Functions as a student portfolio of documentation abilities Offers instructors actual samples of student work fortroubleshooting, notes on each procedure, and procedures for solutionspreparation. PREFACE.ACKNOWLEDGMENTS. TO THE INSTRUCTOR. PART 1: PRELIMINARY EXERCISES. 1. How to Keep a Legally Defensible Laboratory Notebook. 2. Statistical Analysis. 3. Field Sampling Equipment for Environmental Samples. PART 2: EXPERIMENTS FOR AIR SAMPLES. 4. Determination of Henry’s Law Constants. 5. Global Warming: Determining If a Gas Is Infrared Active. 6. Monitoring the Presence of Hydrocarbons in Air around Gasoline Stations. PART 3: EXPERIMENTS FOR WATER SAMPLES. 7. Determination of an Ion Balance for a Water Sample. 8. Measuring the Concentration of Chlorinated Pesticides in Water Samples. 9. Determination of Chloride, Bromide, and Fluoride in Water Samples. 10. Analysis of Nickel Solutions by Ultraviolet–Visible Spectrometry. PART 4: EXPERIMENTS FOR HAZARDOUS WASTE. 11. Determination of the Composition of Unleaded Gasoline Using Gas Chromatography. 12. Precipitation of Metals from Hazardous Waste. 13. Determination of the Nitroaromatics in Synthetic Wastewater from a Munitions Plant. 14. Determination of a Surrogate Toxic Metal in a Simulated Hazardous Waste Sample. 15. Reduction of Substituted Nitrobenzenes by Anaerobic Humic Acid Solutions. PART 5: EXPERIMENTS FOR SEDIMENT AND SOIL SAMPLES. 16. Soxhlet Extraction and Analysis of a Soil or Sediment Sample Contaminated with n-Pentadecane. 17. Determination of a Clay–Water Distribution Coefficient for Copper. PART 6: WET EXPERIMENTS. 18. Determination of Dissolved Oxygen in Water Using the Winkler Method. 19. Determination of the Biochemical Oxygen Demand of Sewage Influent. 20. Determination of Inorganic and Organic Solids in Water Samples: Mass Balance Exercise. 21. Determination of Alkalinity of Natural Waters. 22. Determination of Hardness in a Water Sample. PART 7: FATE AND TRANSPORT CALCULATIONS. 23. pC–pH Diagrams: Equilibrium Diagrams for Weak Acid and Base Systems. 24. Fate and Transport of Pollutants in Rivers and Streams. 25. Fate and Transport of Pollutants in Lake Systems. 26. Fate and Transport of Pollutants in Groundwater Systems. 27. Transport of Pollutants in the Atmosphere. 28. Biochemical Oxygen Demand and the Dissolved Oxygen Sag Curve in a Stream: Streeter–Phelps Equation. APPENDIX A: Periodic Table. INDEX. Frank M. Dunnivant, Elliot Anders ABasic Introduction to Pollutant Fate and Transport: An IntegratedApproach with Chemistry, Modeling, Risk Assessment, and EnvironmentalLegislation http://www.namipan.com/d/57267c52fcc5dff533d00ffcb89fd9d7ed5b62f9163b3e00 [ Last edited by 无机材料 on 2008-11-25 at 14:26 ] |
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