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Full experimental detail for ALL experiments must be provided in supplementary information, with spectroscopic and characterization data. Characterization data must include HRMS (accurate to 0.003 mass units) and/or elemental analysis (accurate to 0.4%) reported individually for ALL new compounds and ALL known compounds where such characterization data is not reported; found and calculated data must be provided.

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Literature references to adequate characterization data (not only to melting points) must be supplied for known compounds, with the relevant experimental data.

Supplementary information must also include copies of 1H and 13C NMR spectra for all new compounds, plus hplc traces, X-ray data, optical rotation data, results of biological testing, and other data as appropriate for key compounds.

You must indicate the availability of supplementary material within your article by adding a paragraph prior to the article¡¯s reference section, e.g., ¡®Supporting Information: Full experimental detail, 1H and 13C NMR spectra, HPLC traces. This material can be found via the ¡°Supplementary Content¡± section of this article¡¯s webpage.¡¯

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