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kuanghua

铜虫 (著名写手)

[求助] 液质联用供试品浓度选择 已有1人参与

对于液质联用进行定性鉴定,供试品浓度一般选择多少或如何判断供试品浓度是否合适?如测定一个相对比较纯的未知杂质的分子量,又或测定供试品中某个未知杂质的分子量等。

咨询工程师的意见说是根据信噪比定,只要信噪比合适就行,但实际上如果仅是信噪比合适,由于质谱检测器灵敏度高,对于未知物鉴定来说,紫外检测器可能就由于浓度低而没有峰了,而浓度大了又担心质谱系统被污染!查了一下论坛,有说按e5或e6次方初步判断,也有说按多少ppm算的,到底如何判断是比较科学合理或简单实用的?

注:实验室液质型号为安捷伦1260-6120B。
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华哥哥

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【答案】应助回帖

看了一些文献,从几十μg/mL到1mg/mL都有人采用,不过还是μg/mL级别的比较多,或者你先用低浓度的试试吧
2楼2016-11-09 16:19:24
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