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7.3 Reference Junction Temperatures¡ªA controlled temperature medium shall be provided in which the temperature of the thermocouple reference junctions is maintained constant during a measurement cycle at a known or measured value. A commonly used reference temperature is 0 ¡ãC (32 ¡ãF), usually realized through use of the ice point, but other temperatures may be used if desired. An acceptable method for utilizing the ice point as a reference junction is given in Practice E 563. Reports of data taken with reference temperatures other than the ice point should be corrected to reflect the results that would have been obtained if the reference junction had been at the ice point. As an alternative, calibration data taken with a reference junction temperature other than the ice point may be reported without correction, but in such cases the calibration report must clearly state the actual reference junction temperature.
The reference junction temperature shall be known or measured with uncertainty less than that expected from the thermocouple calibration, to minimize this temperature variation as a source of error.
7.3.1 Isothermal and Electronic Reference Junction
Compensation¡ªFor the rapid calibration of large numbers of thermocouples, the reference junctions can be made at an isothermal multiterminal strip. This avoids the thermal loading of the ice bath resulting from the large number of thermocouple and copper connecting wires. The temperature and isothermal condition of the strip shall be established and monitored by the use of a separate, reference temperature sensor. The spatial temperature variation across the terminations on the isothermal unit shall be mapped and accounted for. If desired, the thermocouple emf values obtained with use of an isothermal terminal strip may be compensated such that the compensated emf is equivalent to the thermocouple emf created by a thermocouple with reference junctions at 0 ¡ãC (32 ¡ãF). An electronic reference junction compensator accomplishes this task by accurately monitoring the temperature of the reference junctions and adding to the thermocouple emf an additional emf such that the sum is equivalent to the thermocouple emf produced with reference junctions at 0 ¡ãC. The addition of emf to the thermocouple emf may be accomplished through software methods, as well as through addition of an actual emf. To minimize the uncertainty of an electronic reference junction emf as a source of error, the temperature equivalent of the emf produced by the electronic reference junction shall be known and measured with uncertainty less than that expected from the thermocouple calibration. Whatever reference junction technique is used, its uncertainty must be accounted for in the uncertainty of the thermocouple calibration being performed.
7.3.2 Extension of Thermoelements to Reference
Temperature¡ªWhenever possible, the thermoelements under test shall be continuous, extending from the measuring point through the temperature gradient, to the reference junction without any intermediate connections. In cases where this is not possible, several options exist:
7.3.2.1 Matched Thermoelements¡ªAdditional lengths of thermoelement materials from the same wire lots as those being calibrated may be used to extend the device under test to the reference bath. In such circumstances, no additional corrections are required.
7.3.2.2 Thermoelements of the Same Type with Known
Thermoelectric Response, but from a Different Lot¡ªThermoelements being calibrated may be extended using thermoelement materials of the same type as the thermocouple under test. Such materials may be of thermocouple or extension grade, but shall have a known emf versus temperature relationship over the temperature interval to which they will be subjected, and corrections for the deviations of the extension material relative to the material under test over that interval
shall be made. In general, it will be necessary to calibrate the test wire in the temperature range spanned by the extension wire and to measure the temperature of the junctions between
the different materials in order to make this correction. No correction is necessary if both ends of the extension material are at temperatures within 1 ¡ãC (1.8 ¡ãF). It is also acceptable to not apply a correction if the uncertainty budget for the calibration includes an appropriate allowance for temperature variations of the junction between the thermocouple and the extension material, and the calibration report specifies the range of transition junction temperatures for which the calibration is valid. This allowance may be experimentally determined by maintaining the measuring junction of the thermocouple at a fixed temperature, such as 0 ¡ãC, and varying the temperature of the transition junction over a specified range.
7.3.2.3 Thermocouple Connectors¡ªIn all cases where there are junctions between the thermocouple under test and thermocouple lead wires, the temperature variations across the junctions shall be minimized. Thermocouple connectors as described in Specifications E 1684 and E 1129 will introduce no more than 1.1 ¡ãC (2 ¡ãF) error for a 40 ¡ãC (70 ¡ãF) temperature difference across the connector. This error will be proportionately reduced for smaller temperature differences.
7.3.2.4 Circumstances with Small Temperature
Differences¡ªIn special cases where the temperature differences from end-to-end along the length of the wires used to extend a thermocouple for calibration purposes are very small (less than 62 ¡ãC), thermocouple or extension grade wires of matching thermocouple type may be used in calibration circuits without correction.
7.4 Emf-Measuring Instruments¡ªThe choice of a specific instrument to use for measuring the thermocouple emf will depend on the accuracy required of the calibration being performed. Generally the thermocouple emf will be measured using a digital voltmeter. For the highest level of accuracy,
voltmeters shall have a maximum uncertainty no greater than 10-4 times the emf reading and shall have input impedances larger than the thermocouple loop resistance by at least a factor of 104. Reference junction compensation is required for thermocouple measurement with voltmeters. In order to avoid
forming unintended reference junctions at voltmeter terminals whose temperature may be poorly controlled, thermocouples must not be connected directly to the input terminals of voltmeters without the use of appropriate electronic reference junction compensation and connection of the voltmeter to the compensator with untinned copper wires.
7.5 Connecting Wire Assembly¡ªConnecting wires from the reference junction to the voltmeter shall be insulated copper and shall be configured as twisted pairs for wire lengths greater than 0.3 m (1 ft.), to reduce electromagnetic noise pickup. If the environment contains substantial electromagnetic noise, it may also be useful to run the wires in a grounded electrical shield or braided cable. Copper connections should be clean and free from oxides.
7.5.1 Scanner systems may be used to switch between the reference thermometer and the different thermocouples being calibrated. Such switches shall be of rugged construction and designed so that both connecting wires are switched when switching from one thermocouple to the next, leaving thermocouples not in use electrically isolated. All of the scanner switches shall be constructed of the same material and shall be free of extraneous emf production (see Appendix X3). Precautions should be taken to protect the switches from temperature fluctuations due to convection, conduction, or radiation. Scanning performance shall be evaluated to ensure adequate settling time before measurement.
7.5.2 It is preferable to use wire-to-wire connections in calibration circuits, but if terminal blocks are used for convenience, they shall be protected against the development of temperature gradients across the blocks.
7.6 Thermocouple Insulation and Protection Tubes¡ªIn the case where bare wire thermocouples are tested, two-hole insulation tubing may be used to support and electrically insulate the immersed portion of the two bare thermoelements.
Use only insulation material that will not contaminate the thermocouple (for example, clean, high-purity insulators such as 99.8 % aluminum oxide) and that will provide the necessary electrical insulation at the highest temperature of the calibration.
To prevent contamination of thermocouples by residues left by previously tested thermocouples, each insulator shall only be used with thermocouples of one type and the positive and negative thermoelements shall always be inserted in the same bore. The only exceptions allowed are: type R and type S thermocouples may be calibrated in the same insulators, and the thermoelements of type B thermocouples may be mounted in either bore. To avoid unnecessary mass and to minimize axial heat conduction in the region of the measuring junction, the tubing should be relatively thin walled. Bore diameters should provide a loose fit for the thermocouple wires. During the test, the thermocouples may be inserted in a protection tube that is resistant to thermal shock, and noncontaminating to the thermocouple materials.
7.6.1 Sheathed thermocouples may be tested without further protection or support in liquid or dry fluidized baths, provided that the bath medium is compatible with the sheath material.
Thermocouples insulated with fibrous insulation must not be immersed directly into any bath liquid. Care must be taken to keep thermal conduction losses within the limits of experimental error typically by immersing the thermocouple into the bath until no further indication in temperature change is noted.

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