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xianyun414木虫 (小有名气)
司令
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[求助]
铜纳米线 夏幼南法 已有3人参与
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夏幼南发表在Angew. Chem. Int. Ed. 2011, 50, 10560 –10564的文章，制备铜纳米线是在22.2ml Vial,这在100摄氏度加热下会不会把瓶盖给冲出来，或者爆了，可以在三口烧瓶里进行反应吗，还是说反应本身须在一定的压力下进行呢。以下为反应条件，谢谢 All the chemicals were obtained from Sigma-Aldrich and used as received. In a standard synthesis of Cu nanowires, 21 mg CuCl2·2H2O, 180 mg HDA, and 50 mg glucose (α or form) were dissolved in 10 mL water in a 22.2-mL vial (borosilicate glass vial, with a black phenolic molded screw cap and polyvinyl-faced pulp liner, VWR International, Radnor, PA) at room temperature. After the vial had been capped, the solution was magnetically stirred at room temperature overnight. The capped vial was then transferred into an oil bath and heated at 100 oC for 6 h under magnetic stirring. |
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