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13CNMR(101MHz,MeOD)δ20.7,25.6,28.7,43.2,64.4,69.3,71.6,71.7,74.9,75.1,75.3,75.5,75.9,78.7,96.7,97.0,97.6,105.7,105.8,113.5,118.6,120.5,120.7,121.1,121.2,122.3,130.8,132.6,132....

13CNMR(101MHz,D2O)δ24.0,26.5,31.9,38.8,41.6,43.4,51.8,51.9,59.8,60.7,69.3,69.5,72.5,72.6,75.5,75.6,76.2,97.2,97.3,98.2,98.9,104.6,110.3,119.6,120.7,131.3,133.7,152.6,153.2,169...

13CNMR(101MHz,MeOD)δ13.3,19.3,25.6,28.1,28.7,43.3,51.8,57.7,62.4,64.1,64.3,65.6,69.1,69.6,70.9,71.1,71.3,71.5,72.7,72.9,73.1,73.4,73.8,74.3,74.6,75.9,76.0,77.5,77.6,77.6,77.9,...

13CNMR(101MHz,CDCl3)δ7.4,9.5,17.6,18.6,18.9,21.4,21.6,27.1,27.3,27.7,36.7,38.6,43.4,45.3,47.0,48.6,52.4,55.7,56.6,67.6,69.3,70.7,82.8,84.7,105.9,120.9,127.8,129.9,154.4,195.4,...

13CNMR(101MHz,MeOD)δ13.7,14.2,19.3,20.0,28.4,35.7,41.1,43.7,45.2,51.9,62.7,69.8,71.5,74.6,77.9,79.4,97.7,99.6,100.1,111.4,121.1,133.2,135.6,153.7,154.0,169.3.LF-65

13CNMR(101MHz,D2O)δ28.5,36.7,42.3,43.5,63.3,63.9,67.6,69.5,71.4,74.1,75.4,75.7,75.9,76.2,95.9,96.5,96.9,98.1,115.5,120.2,120.8,131.9,133.0,145.9,180.5LF-63谢谢

13CNMR(101MHz,D2O)δ29.1,37.6,43.7,51.8.60.6,69.5,72.5,72.6,75.4,75.5,76.1,76.2,97.0,98.2,98.6,109.8,120.2,132.7,152.3,169.5.

13CNMR(101MHz,MeOD)δ171.23,171.13,170.83,169.45,169.13,168.77,168....71.48,71.22,69.66,69.34,65.11,62.69,62.42,61.09,51.87,51.81,45.24,43.70,43.09,33.66,28.63,28.34,25.83,13.76.

13CNMR(101MHz,MeOD)δ11.5,19.4,19.5,29.9,40.3,41.0,45.1,60.7,61.4,62.3,63.0,69.4,70.0,70.8,71.6,71.8,72.0,73.2,73.3,73.7,73.8,74.2,76.3,76.9,77.2,78.1,78.2,95.7,96.4,101.5,104....