|
|
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
沐风14: 金币+20 2015-06-29 20:44:55
PDF#34-1266: QM=Star(S); d=Diffractometer; I=Diffractometer
Akaganeite-Q, syn
Fe +3 O ( O H )
Radiation=CoKa Lambda=1.7902 Filter=Graph
Calibration= 2T=11.842-64.396 I/Ic(RIR)=
Ref: Murad, E.
Clay Miner., v14 p273 (1979)
Tetragonal - (Unknown), I4/m (87) Z=8 mp=
CELL: 10.535 x 10.535 x 3.03 <90.0 x 90.0 x 90.0> P.S=tI32 (?)
Density(c)=3.512 Density(m)=3.86A Mwt=88.85 Vol=336.29 F(24)=47.3(.0195,26/0)
Ref: Ibid.
Strong Lines: 3.33/X 2.55/6 7.47/4 2.30/4 1.64/4 5.28/3 2.63/3 1.95/2 1.76/2 1.45/2
NOTE: A 0.1M Fe Cl3 solution was heated to 60 C for 8 days.
The precipitate was separated by centrifuging, washed with H2 O and dried at 40 C.
To replace 00-013-0157.
2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2
11.842 7.4670 40.0 ( 1 1 0) 5.921 0.0670 0.8415
16.790 5.2760 30.0 ( 2 0 0) 8.395 0.0948 1.1909
23.849 3.7280 5.0 ( 2 2 0) 11.924 0.1341 1.6854
26.725 3.3330 100.0 ( 3 1 0) 13.362 0.1500 1.8851
34.003 2.6344 25.0 ( 4 0 0) 17.001 0.1898 2.3851
35.161 2.5502 55.0 ( 2 1 1) 17.581 0.1961 2.4638
36.145 2.4830 2.0 ( 3 3 0) 18.073 0.2014 2.5305
38.168 2.3559 9.0 ( 4 2 0) 19.084 0.2122 2.6670
39.219 2.2952 35.0 ( 3 0 1) 19.609 0.2178 2.7375
42.955 2.1038 7.0 ( 3 2 1) 21.478 0.2377 2.9866
43.768 2.0666 7.0 ( 5 1 0) 21.884 0.2419 3.0403
46.433 1.9540 20.0 ( 4 1 1) 23.217 0.2559 3.2156
48.862 1.8624 4.0 ( 4 4 0) 24.431 0.2685 3.3737
50.457 1.8072 <1 ( 5 3 0) 25.228 0.2767 3.4768
52.046 1.7557 15.0 ( 6 0 0) 26.023 0.2848 3.5787
52.882 1.7299 3.0 ( 4 3 1) 26.441 0.2890 3.6321
55.085 1.6658 <1 ( 6 2 0) 27.543 0.3002 3.7719
55.901 1.6434 35.0 ( 5 2 1) 27.951 0.3042 3.8233
61.097 1.5155 9.0 ( 0 0 2) 30.549 0.3299 4.1459
61.642 1.5034 5.0 ( 6 1 1) 30.821 0.3326 4.1793
62.277 1.4896 3.0 ( 7 1 0) 31.138 0.3357 4.2180
62.482 1.4852 3.0 ( 1 1 2) 31.241 0.3367 4.2305
63.798 1.4577 1.0 ( 2 0 2) 31.899 0.3430 4.3103
64.396 1.4456 15.0 ( 5 4 1) 32.198 0.3459 4.3464 |
|
点击这里搜索更多相关资源
回复此楼