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[求助]
微谱求助,十分感激! 已有1人参与
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碳谱数据为211.1,211.0,177.2,171.1,170.8,144.8,123.2,105.4,105.1,104.9,104.6,104.0,103.8,101.7,101.6,95.4,86.5,86.4,85.3,83.0,80.8,78.8,78.8,78.6,78.3,78.2,78.0,77.8,77.5,76.9,76.7,76.5,76.3,76.0,75.7,75.4,75.3,75.2,75.1,74.8,74.8,73.8,73.6,73.5,72.8,72.7,71.4,71.4,71.3,71.3,71.2,71.2,71.0,70.8,70.5,69.1,67.2,67.0,62.4,62.2,56.2,56.2,56.1,56.1,54.7,52.9,52.8,49.9,49.5,48.1,48.0,42.7,42.3,41.1,39.2,37.1,36.5,33.7,33.4,31.9,31.3,27.3,25,7,25.6,24.9,24.5,21.4,,17.8,16.5,16.3,11.0,10.9 溶剂为甲醇,估计为齐敦果烷型三萜皂苷类化合物,非常谢谢! |
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【答案】应助回帖
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978412600: 金币+40, ★有帮助, 非常感谢! 2015-04-13 15:45:43
感谢参与,应助指数 +1
978412600: 金币+40, ★有帮助, 非常感谢! 2015-04-13 15:45:43
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1 . compound 22 相似度:75.2% Phytochemistry 2000 55 419-428 Structural studies of triterpenoid saponins with new acyl components from Quillaja saponaria Molina Shengjun Guo, Lennart Kenne Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . compound S11 相似度:72.3% Carbohydrate Research 2000 329 817-829 Novel acetylated triterpenoid saponins in a chromatographic fraction from Quillaja saponaria Molina Lars I. Nord, Lennart Kenne Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . compound S8 相似度:72.0% Carbohydrate Research 2000 329 817-829 Novel acetylated triterpenoid saponins in a chromatographic fraction from Quillaja saponaria Molina Lars I. Nord, Lennart Kenne Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . compound S12 相似度:72.0% Carbohydrate Research 2000 329 817-829 Novel acetylated triterpenoid saponins in a chromatographic fraction from Quillaja saponaria Molina Lars I. Nord, Lennart Kenne Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . compound S7 相似度:70.9% Carbohydrate Research 2000 329 817-829 Novel acetylated triterpenoid saponins in a chromatographic fraction from Quillaja saponaria Molina Lars I. Nord, Lennart Kenne Structure 13C NMR Structure & 13C NMR 碳谱模拟图 6 . crocosmioside G C96H158O48 相似度:67.7% Chemical & Pharmaceutical Bulletin 1990 38 142-149 Novel Acylated Saponins from Montbretia (Crocosmia crocosmiiflora). II. : The Structures of Crocosmiosides C, D, E, F, G and I Yoshihisa ASADA,Takehito UEOKA and Tsutomu FURUYA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 7 . masonoside A 相似度:66.6% Phytochemistry 1994 35 757-764 Acylated saponins, masonosides A–C, from the corms of Crocosmia masoniorum Yoshihisa Asada, Masako Ikeno, Tsutomu Furuya Structure 13C NMR Structure & 13C NMR 碳谱模拟图 8 . desacylmasonorida 1 相似度:66.6% Phytochemistry 1994 35 757-764 Acylated saponins, masonosides A–C, from the corms of Crocosmia masoniorum Yoshihisa Asada, Masako Ikeno, Tsutomu Furuya Structure 13C NMR Structure & 13C NMR 碳谱模拟图 9 . calliandra saponin B C92H147NO45 相似度:65.5% Chemical & Pharmaceutical Bulletin 1994 42 1111-1115 Studies on the Constituents of Calliandra anomala (KUNTH) MACBR. II. Structure Elucidation of Four Acylated Triterpenoidal Saponins Takatoshi NAKAMURA,Tadahiro TAKEDA and Yukio OGIHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 10 . crocosmioside C C90H148O44 相似度:65.5% Chemical & Pharmaceutical Bulletin 1990 38 142-149 Novel Acylated Saponins from Montbretia (Crocosmia crocosmiiflora). II. : The Structures of Crocosmiosides C, D, E, F, G and I Yoshihisa ASADA,Takehito UEOKA and Tsutomu FURUYA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 11 . crocosmioside F C91H152O44 相似度:65.5% Chemical & Pharmaceutical Bulletin 1990 38 142-149 Novel Acylated Saponins from Montbretia (Crocosmia crocosmiiflora). II. : The Structures of Crocosmiosides C, D, E, F, G and I Yoshihisa ASADA,Takehito UEOKA and Tsutomu FURUYA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 12 . masonoside A 相似度:65.5% Phytochemistry 1994 35 757-764 Acylated saponins, masonosides A–C, from the corms of Crocosmia masoniorum Yoshihisa Asada, Masako Ikeno, Tsutomu Furuya Structure 13C NMR Structure & 13C NMR 碳谱模拟图 13 . crocosmioside D C90H150O44 相似度:64.5% Chemical & Pharmaceutical Bulletin 1990 38 142-149 Novel Acylated Saponins from Montbretia (Crocosmia crocosmiiflora). II. : The Structures of Crocosmiosides C, D, E, F, G and I Yoshihisa ASADA,Takehito UEOKA and Tsutomu FURUYA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 14 . Clematochinenoside G C92H142O48 相似度:64.5% Journal of Natural Products 2010 73 1234-1239 Triterpene Saponins from Clematis chinensis and Their Potential Anti-inflammatory Activity Qiang Fu, Ke Zan, Mingbo Zhao, Sixiang Zhou, Shepo Shi, Yong Jiang and Pengfei Tu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 15 . compound 1 C96H143NO43 相似度:63.8% Journal of Natural Products 2006 69 1323-1329 Antiproliferative Triterpene Saponins from Entada africana Giuseppina Cioffi, Fabrizio Dal Piaz, Paolo De Caprariis, Rokia Sanogo, Stefania Marzocco, Giuseppina Autore, and Nunziatina De Tommasi Structure 13C NMR Structure & 13C NMR 碳谱模拟图 16 . Clematochinenoside B C94H154O54 相似度:63.8% Journal of Natural Products 2010 73 1234-1239 Triterpene Saponins from Clematis chinensis and Their Potential Anti-inflammatory Activity Qiang Fu, Ke Zan, Mingbo Zhao, Sixiang Zhou, Shepo Shi, Yong Jiang and Pengfei Tu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 17 . calliandra saponin A 相似度:63.4% Chemical & Pharmaceutical Bulletin 1994 42 1111-1115 Studies on the Constituents of Calliandra anomala (KUNTH) MACBR. II. Structure Elucidation of Four Acylated Triterpenoidal Saponins Takatoshi NAKAMURA,Tadahiro TAKEDA and Yukio OGIHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 18 . calliandra saponin A C91H145NO45 相似度:63.4% Chemical & Pharmaceutical Bulletin 1993 41 2132-2137 Studies on the Constituents of Calliandra anomala (KUNTH) MACBR. I. Structure Elucidation of Two Acylated Triterpenoidal Saponins Tadahiro TAKEDA,Takatoshi NAKAMURA,Shigeki TAKASHIMA,Osamu YANO and Yukio OGIHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 19 . crocosmioside A C90H150O43 相似度:63.4% Chemical & Pharmaceutical Bulletin 1989 37 2139-2146 Novel Acylated Saponins from Montbretia (Crocosmia crocosmiiflora). Isolation of Saponins and the Structures of Crocosmiosides A, B and H Yoshihisa ASADA,Takehito UEOKA and Tsutomu FURUYA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 20 . (E/Z)-Polygalasaponin XLIV 相似度:63.4% Natural Product Research and Development 2011 23 670-674 Isolation and Identification of Saponins from Polygala crotalarioides ZHOU, Fan-rui, WANG, Jun-min, ZHOU, Xiao, HUA, Yan Structure 13C NMR Structure & 13C NMR 碳谱模拟图 21 . Clematiunicinoside G C88H144O48 相似度:63.4% Chemical & Pharmaceutical Bulletin 2014 62 35-44 Triterpenoid Saponins from the Roots of Clematis uncinata Shuo-Guo Li, Xiao-Jun Huang, Man-Mei Li, Mei Wang, Rui-Bing Feng, Wei Zhang, Yao-Lan Li, Ying Wang, Wen-Cai Ye Structure 13C NMR Structure & 13C NMR 碳谱模拟图 22 . 3-O-β-D-glucopyranosylpresenegenin 28-O-β-D-galactopyranosyl-(1→4)-β-D-xylopyranosyl-(1→4)-α-L-rhamnopyranosyl-(1→2)-[6-O-acetyl-β-D-glucopyranosyl-(1→3)]-{ 4-O-[(E/Z)-3,4-dimethoxycinnamoyl]}-β-D-fucopyranosyl ester 相似度:63.1% Natural Product Research and Development 2011 23 670-674 Isolation and Identification of Saponins from Polygala crotalarioides ZHOU, Fan-rui, WANG, Jun-min, ZHOU, Xiao, HUA, Yan Structure 13C NMR Structure & 13C NMR 碳谱模拟图 23 . gleditsia saponin C C94H148O43 相似度:62.7% Chemical & Pharmaceutical Bulletin 1999 47 388-393 Triterpenoidal Saponins Acylated with Two Monoterpenic Acids from Gleditsia sinensis Zhizhen ZHANG,Kazuo KOIKE,Zhonghua JIA,Tamotsu NIKAIDO,Dean GUO and Junhua ZHENG Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
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