10楼: Originally posted by Picat at 2015-01-14 13:47:19
哦这个倒没研究过，只是觉得方法好用，能重复。...

6楼: Originally posted by Picat at 2015-01-13 15:12:36
水热法请参考 (Angew. Chem. Int. Ed., 10.1002/anie.200901566)：
Typically, FeCl3 (0.65 g, 4.0 mmol) and trisodium citrate (0.20 g, 0.68 mmol) were first dissolved in
ethylene glycol (20 mL), afterwa ...

12楼: Originally posted by 千军万马wcw at 2015-01-26 20:33:47
您说的第一种方法文献不对吧，为什么问我下下来事一篇综述？您能再确定下吗...

5楼: Originally posted by 默默修炼 at 2015-01-09 21:57:18
合成Fe3O4方法很多，最经典的是共沉淀法，但是由于反应温度为常温，合成的纳米粒结晶度不够，饱和磁化强度也不好。现在合成粒径和形貌兼优的主流方法为高温分解法和水热法，高温分解法查阅孙守恒的文献，水热法查阅 ...