6楼: Originally posted by zhanhf13 at 2014-11-04 11:05:55
单体蒸馏提纯了没，温度是不是太高，pH调节，水中除氧了没

7楼: Originally posted by caibb67 at 2014-11-04 11:23:51
看不懂什么意思

10楼: Originally posted by 曹冬灵Aling at 2014-11-05 08:30:51
我这个实验做过七八次了，主要感觉是引发剂浓度的问题，之前浓度太高，直接结块了...

8楼: Originally posted by 曹冬灵Aling at 2014-11-05 15:28:00
没有乳化剂，只是两者的反应，我们主要想得到的是改性后的聚苯乙烯乳液...

13楼: Originally posted by xvxv at 2014-11-05 22:10:31
引发剂加单体的1 wt% 以下都行...

14楼: Originally posted by lubo608 at 2014-11-06 07:43:35
不加乳化剂怎么会得到乳液？无乳化剂乳液聚合也不是这么做的。...

16楼: Originally posted by 曹冬灵Aling at 2014-11-06 21:11:29
我们是根据资料做的，无皂乳液聚合。http://wenku.baidu.com/link?url=zvME12WFdDE81ivup5s2n8kaGmYkdllByaWCvHDpCsq-etFWpInEnK3u53FUzUCvisHv8gg7rQaz9Y9TtAETCfBN0psRqYdU30OqH_N7dty 就是这篇文章...

17楼: Originally posted by lubo608 at 2014-11-06 22:22:33
无皂乳液聚合是用聚甲基丙烯酸盐代替乳化剂，你的配方没提到用聚甲基丙烯酸盐。...