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ÀýÈçSynthesis of ZnO NW films. A typical procedure for synthesizing the ZnO NW films is carried out as in the literature [29]. Firstly, a seed layer was deposited on the conductive F-doped SnO2 (FTO) glass by sol¨Cgel method using the zinc acetate dihydrate (Zn(Ac)2¡¤2H2O, 0.5 mol L−1) as the precursor and then the substrates coated with ZnO seed layer were calcined at 500 ◦C for 1 h. The precursor aqueous solution for the growth of ZnO NW was prepared in advance by mixing the hexamethylenetetramine (HMT, 0.025 mol L−1) and Zn(Ac)2¡¤2H2O (0.025 mol L−1) in deionized water, and stirring for 20 min at 0 ◦C. Then the FTO substrates with ZnO seed layer were immersed into this solution immediately and sealed in a flask in an oven at 95 ◦C for 7 h. Then the films were rinsed in deionized water thoroughly and subsequently heated at 500 ◦C for 1 h. The film obtained in this step was marked as ZNW¡£Journal of Photochemistry and Photobiology A: Chemistry 219 (2011) 132¨C138¡£µÚÒ»²½¾ÍÊǾ§ÖÖ |
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3Â¥2013-12-08 21:24:52
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