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ontaii

木虫 (小有名气)

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专业: 无机合成和制备化学

【答案】应助回帖

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蓝胖胖f: 金币+8, ★★★很有帮助 2013-10-14 10:22:06

引用回帖:

10楼: Originally posted by 蓝胖胖f at 2013-10-12 16:35:43
非常感谢你的分析，可以提供相关文献吗？

...

J. Electrochem. Soc. 2012, Volume 159, Issue 5, Pages J193-J199.

It is worth mentioning that, we have tried several heating conditions ranging from 1000◦C to 1600◦C to prepare MgY4Si3O13-based phosphors. All the samples are found to have impure MgY4Si3O13 -phase below 1300◦C, while monophasic nature with more defined PXRD patterns were clearly seen in the samples synthesized at 1500◦C as presented in Fig. 1......

根本不需要讲那么多直接把合成条件写在论文里面就够了

赞一下

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11楼2013-10-12 20:55:44

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

蓝胖胖f

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引用回帖:

11楼: Originally posted by ontaii at 2013-10-12 20:55:44
J. Electrochem. Soc. 2012, Volume 159, Issue 5, Pages J193-J199.

It is worth mentioning that, we have tried several heating conditions ranging from 1000◦C to 1600◦C to prepare MgY4Si3 ...

非常感谢