| 查看: 6061 | 回复: 15 | ||||
[交流]
求助Al2p的XPS分析 已有4人参与
|
||||
| 小弟在分析複合薄膜,當中含有Cr,Al,N,O成份。但在Al2p分峰時出現兩個峰,位置分別在73.78及76.79,不知道是73.78到底是Al-Al BOND還是Al-O,還有就是另一個峰到底是那一種結合物。望各路高手給點提示,感激不盡! |
回复此楼» 猜你喜欢
求助一篇MEMS散热器件文献
已经有0人回复
-
材化专业SCI论文（职称评定）
已经有0人回复
-
无机化学论文润色/翻译怎么收费?
已经有224人回复
-
材料化学专业SCI论文（职称评定）
已经有0人回复
» 本主题相关价值贴推荐，对您同样有帮助:
- XPS数据分析求助！！万分感谢！怎么我的求助帖没人回复呢，有重金啊！
已经有15人回复
- X射线光电子能谱 XPS数据分析求助！！急！万分感谢！
已经有8人回复
- 再次求助分析XPS
已经有12人回复
- 求助XPS PEAKFIT软件（谢谢！）
已经有18人回复
- 求助。。。铜的XPS分析
已经有9人回复
- xps图谱分析求助
已经有4人回复
- 【求助】XPS价态分析（Mo）
已经有16人回复
- 【求助】关于XPS与EDS的区别
已经有8人回复
- 【求助】Mo的XPS分析【麻烦大家了】
已经有16人回复
- 【求助】XPS数据分析
已经有6人回复
- 【求助】XPS拟合软件及方法
已经有12人回复
- 【求助】如何通过两种元素的XPS结果来分析元素比例?
已经有12人回复
- 【求助】XPS 谱图分析
已经有10人回复
- 【求助】关于XPS谱图中FWHM
已经有5人回复
fds329
荣誉版主 (文坛精英)
鱼大婶
-
专家经验: +1536 - 应助: 207 (大学生)
- 贵宾: 6.842
- 金币: 59179.4
- 散金: 21817
- 红花: 261
- 沙发: 156
- 帖子: 46404
- 在线: 2171.7小时
- 虫号: 538323
- 注册: 2008-04-02
- 专业: 无机化学
- 管辖: 无机/物化
2楼2013-02-04 21:39:54
fds329
荣誉版主 (文坛精英)
鱼大婶
-
专家经验: +1536 - 应助: 207 (大学生)
- 贵宾: 6.842
- 金币: 59179.4
- 散金: 21817
- 红花: 261
- 沙发: 156
- 帖子: 46404
- 在线: 2171.7小时
- 虫号: 538323
- 注册: 2008-04-02
- 专业: 无机化学
- 管辖: 无机/物化
★ ★ ★
小木虫: 金币+0.5, 给个红包，谢谢回帖
yanhualover: 金币+2, 谢谢提供数据。优秀参与，值得奖励。 2013-02-06 00:58:43
小木虫: 金币+0.5, 给个红包，谢谢回帖
yanhualover: 金币+2, 谢谢提供数据。优秀参与，值得奖励。 2013-02-06 00:58:43
|
可以查文献看。下面是美国标准及参考文献 Element: Al Formula: Al0.7Cr1.3ZnS4 Name: aluminum chromium sulfur zinc ss Classes: solid solution Author Name(s): Battistoni C., Paparazzo E., Dumond Y., Nogues M. Journal: Solid State Commun. 46, 333 (1983) Data Type: Photoelectron Line Line Designation: 2p3/2 Binding Energy (eV) 73.8 Element: Al Formula: Al2O3.3H2O XPS Formula: Al*2O3.3H2O Name: dialuminum(III) trioxide trihydrate (gibbsite) CAS Registry No: 14762-49-3 Classes: hydrate, mineral, oxide Author Name(s): Sugama T., KuKacka L.E., Carciello N., Hocker N.J. Journal: Cement and Concrete Research 19, 857 (1989) Data Type: Photoelectron Line Line Designation: 2p3/2 Quality of Data: Adequate Binding Energy (eV) 73.8 Element: Al Formula: Y3Al5O12 XPS Formula: Y3Al*5O12 Name: triyttrium(III) pentaaluminum(III) dodecaoxide Classes: double oxide Author Name(s): Mullins W.M., Averbach B.L. Journal: Surf. Sci. 206, 29 (1988) Data Type: Photoelectron Line Line Designation: 2p3/2 Quality of Data: Adequate Binding Energy (eV) 73.77 Background Subtraction Method: other Peak Location Method: Gaussian General: Element: Al Formula: Al2O3 Name: aluminum(III) oxide CAS Registry No: 1344-28-1 Classes: anhydride, oxide Author Name(s): Kovacich J.A., Lichtman D. Journal: J. Electron Spectrosc. Relat. Phenom. 18, 341 (1980) Data Type: Photoelectron Line Line Designation: 2p3/2 Binding Energy (eV) 73.7 Measurement Information: Use of X-ray Monochromator: No Calibration: Cu3s=122.4;2p3=932.5 Charge Reference: Adventitious carbon Energy Scale Evalution: Reliable, with two-point correction of energy scale Element: Al Formula: Al2O3 Name: aluminum(III) oxide CAS Registry No: 1344-28-1 Classes: anhydride, oxide Author Name(s): Wagner C.D., Passoja D.E., Hillery H.F., Kinisky T.G., Six H.A., Jansen W.T., Taylor J.A. Journal: J. Vac. Sci. Technol. 21, 933 (1982) Data Type: Photoelectron Line Line Designation: 2p3/2 Binding Energy (eV) 73.72 Measurement Information: Use of X-ray Monochromator: No Calibration: Au,Cu Charge Reference: Adventitious carbon Energy Scale Evalution: Reliable, with two-point correction of energy scale Element: Al Formula: Al25Ni75Ox XPS Formula: Al*2O3 intermediate Name: aluminum nickel alloy(25-75) oxides Classes: alloy, non-stoichiometric oxide Author Name(s): Venezia A.M., Loxton C.M. Journal: Surf. Sci. 194, 136 (1988) Data Processing: Data Type: Photoelectron Line Line Designation: 2p3/2 Quality of Data: Adequate Binding Energy (eV) 73.76 Energy Uncertainty: 0.08 Background Subtraction Method: other Peak Location Method: other type of curve fit Full Width at Half-maximum Intensity (eV): 2.0 Measurement Information: Use of X-ray Monochromator: No Excitation Energy: Mg Calibration: Au4f7 = 84.00 Charge Reference: Conductor Energy Scale Evalution: Reliable, with one-point correction of energy scale Specimen: oxygen pressure, oxidizing atmosphere, thermal oxide Specimen Temperature (K): 293 Sample Quality: Adequate Notes: Specimens were exposed by 300 L O2 at 773 K. The Ni 3p3/2 binding energy was used as a secondary binding energy reference and was assigned a value of 66.08 eV. |
3楼2013-02-04 21:45:12
鹰羽龙
木虫 (著名写手)
- 应助: 141 (高中生)
- 金币: 3479.1
- 散金: 1499
- 红花: 13
- 帖子: 1267
- 在线: 956.4小时
- 虫号: 369935
- 注册: 2007-05-13
- 性别: GG
- 专业: 理论和计算化学
JJLuNgJJ10楼2013-02-07 21:03:25
4楼2013-02-05 23:12:15
鹰羽龙
木虫 (著名写手)
- 应助: 141 (高中生)
- 金币: 3479.1
- 散金: 1499
- 红花: 13
- 帖子: 1267
- 在线: 956.4小时
- 虫号: 369935
- 注册: 2007-05-13
- 性别: GG
- 专业: 理论和计算化学
5楼2013-02-06 13:42:59
6楼2013-02-07 01:16:16
fds329
荣誉版主 (文坛精英)
鱼大婶
-
专家经验: +1536 - 应助: 207 (大学生)
- 贵宾: 6.842
- 金币: 59179.4
- 散金: 21817
- 红花: 261
- 沙发: 156
- 帖子: 46404
- 在线: 2171.7小时
- 虫号: 538323
- 注册: 2008-04-02
- 专业: 无机化学
- 管辖: 无机/物化
7楼2013-02-07 07:34:33
8楼2013-02-07 14:31:45
9楼2013-02-07 14:35:10
