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ncyxoy木虫 (正式写手)
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[求助]
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title：An HPLC method for the determination of auraptene in dog plasma: application to pharmacokinetic study. Author： Li, Ming; Yuan, Jinbin; Chen, Heifang; Yang, Journal: Latin American Journal of Pharmacy; 2012，vol. 31, no. 02 ，251-256 求该篇论文的检索号，哪位高手能提供？ |
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chenggong6768
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ncyxoy4楼2012-06-30 17:10:22
ncyxoy
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【答案】应助回帖
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ncyxoy: 金币+6, ★★★很有帮助, 谢谢你的应助！ 2012-07-03 17:45:40
ncyxoy: 金币+6, ★★★很有帮助, 谢谢你的应助！ 2012-07-03 17:45:40
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Simultaneous quantification of polymethoxylated flavones and coumarins in Fructus aurantii and Fructus aurantii immaturus using HPLC-ESI-MS/MS 作者: Chen, HF (Chen, Hai-Fang)1; Zhang, WG (Zhang, Wu-Gang)2; Yuan, JB (Yuan, Jin-Bin)1; Li, YG (Li, Yan-Gang)1; Yang, SL (Yang, Shi-Lin)2; Yang, WL (Yang, Wu-Liang)1 来源出版物: JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS 卷: 59 页: 90-95 DOI: 10.1016/j.jpba.2011.10.013 出版年: FEB 5 2012 被引频次: 0 (来自 Web of Science) 引用的参考文献: 18 [ 查看 Related Records ] 引证关系图 摘要: The major lipid-soluble constituents in Fructus aurantii (zhiqiao) and Fructus aurantii immaturus (zhishi) are polymethoxylated flavones (PMFs) and coumarins. In the present study, a high-performance liquid chromatography with electrospray ionization tandem mass spectrometry method was developed to quantify PMFs (nobiletin, tangeretin, 5-hydroxy-6,7,8,4'-tetramethoxyflavone, and natsudaidai) and coumarins (marmin, meranzin hydrate, and auraptene) simultaneously. PMFs and coumarins were detected by electrospray ionization tandem mass spectrometry in positive ion mode and quantified with multiple reaction monitor. Samples were separated on a Diamonsil C(18) (150 mm x 4.6 mm, 5 mu m) column using acetonitrile and formic acid-water solution as a mobile phase in gradient mode with a flow rate at 0.5 mL/min. All calibration curves showed good linearity (r(2) > 0.9977) within the test ranges. Variations of the intraday and interday precisions were less than 4.07%. The recoveries of the components were within the range of 95.79%-105.04% and the relative standard deviations were less than 3.82%. The method developed was validated with acceptable accuracy, precision, and extraction recoveries and can be applied for the identification and quantification of four PMFs and three coumarins in citrus herbs. (C) 2011 Elsevier B.V. All rights reserved. 入藏号: WOS:000297716500012 文献类型: Article 语种: English 作者关键词: Polymethoxylated flavones; Coumarin; Citrus; HPLC-ESI-MS/MS; Quantification KeyWords Plus: PERFORMANCE LIQUID-CHROMATOGRAPHY; OXYGEN HETEROCYCLIC-COMPOUNDS; CITRUS ESSENTIAL OILS; HYDROXYLATED POLYMETHOXYFLAVONES; MASS-SPECTROMETRY; CELL-LINES; IDENTIFICATION; NOBILETIN; MARMIN 通讯作者地址: Yang, WL (通讯作者),Jiangxi Univ Tradit Chinese Med, Key Lab Modern Preparat TCM, Minist Educ, Nanchang 330004, Jiangxi, Peoples R China 地址: 1. Jiangxi Univ Tradit Chinese Med, Key Lab Modern Preparat TCM, Minist Educ, Nanchang 330004, Jiangxi, Peoples R China 2. Jiangxi Univ Tradit Chinese Med, Natl Pharmaceut Engn Ctr Solid Preparat Chinese H, Nanchang 330004, Jiangxi, Peoples R China 电子邮件地址: yangwuliang@163.com 基金资助致谢: 基金资助机构 授权号 Important National Science & Technology Specific Projects 2009ZX09103-350 NSFC 30660230 [显示基金资助信息][隐藏基金资助信息] This work was supported by Important National Science & Technology Specific Projects (2009ZX09103-350), NSFC (30660230). 出版商: ELSEVIER SCIENCE BV, PO BOX 211, 1000 AE AMSTERDAM, NETHERLANDS Web of Science 分类: Chemistry, Analytical; Pharmacology & Pharmacy 学科类别: Chemistry; Pharmacology & Pharmacy IDS 号: 857KD ISSN: 0731-7085 |
7楼2012-07-03 17:00:06
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