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mater_sh银虫 (小有名气)
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[求助]
帮忙NbC和NbN的PDF卡
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| 请各位，做了个X射线，想求助NbC 和NbN的x射线PDF卡。谢谢各位！ |
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3楼2011-05-17 10:58:45
【答案】应助回帖
mater_sh(金币+3): 谢谢您的帮助，但是由于下面还有一个，所以给你3分。别介意。呵呵。 2011-05-21 17:14:47
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PDF#38-1364: QM=Star(+); d=Diffractometer; I=Diffractometer Niobocarbide, syn Nb C (Black) Radiation=CuKa1 Lambda=1.5405981 Filter=Graph Calibration=Internal(Si) d-Cutoff=17.7 I/Ic(RIR)= Ref= Wong-Ng, W., McMurdie, H., Paretzkin, B., Hubbard, C., Dragoo, A., NBS, Gaithersburg, MD, USA. ICDD Grant-in-Aid (1986) Cubic - Powder Diffraction, Fm-3m (225) Z=4 mp= Cell=4.4698 Pearson=cF8 (Cl Na) Density(c)=7.804 Density(m)=8.10A Mwt=104.92 Vol=89.30 F(10)=137.0(.0073,10) Ref= Wong-Ng, W., McMurdie, H., Paretzkin, B., Hubbard, C., Dragoo, A. Powder Diffraction, 3 55 (1988) Strong Line: 2.58/X 2.24/8 1.58/4 1.35/3 1.00/1 1.29/1 1.03/1 0.91/1 0.86/1 1.12/1 NOTE: The mean temperature of the data collection was 25.5 C. The structure of NbC was determined by Rudy et al. (1). The sample was from Alfa Products, Danvers, Massachusetts, USA. To replace 00-010-0181. Spectroscopic analysis indicated impurities of Ta 0.02%, Ti 0.01%, and Fe 0.07%. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 2.5809 100.0 100.0 1 1 1 3 34.730 17.365 0.1937 2.4345 2.2352 80.0 92.0 2 0 0 4 40.316 20.158 0.2237 2.8110 1.5804 35.0 57.0 2 2 0 8 58.337 29.169 0.3164 3.9756 1.3477 26.0 50.0 3 1 1 11 69.718 34.859 0.3710 4.6622 1.2903 9.0 18.0 2 2 2 12 73.306 36.653 0.3875 4.8695 1.1176 5.0 12.0 4 0 0 16 87.139 43.569 0.4474 5.6221 1.0253 7.0 18.0 3 3 1 19 97.401 48.701 0.4877 6.1281 0.9994 10.0 26.0 4 2 0 20 100.841 50.420 0.5003 6.2869 0.9124 7.0 20.0 4 2 2 24 115.179 57.589 0.5480 6.8864 0.8603 6.0 18.0 5 1 1 27 127.121 63.561 0.5812 7.3038 PDF#14-0547: QM=Doubtful(?); d=(Unknown); I=Film/Visual Niobium Nitride Nb N Radiation=CuKa Lambda=1.5418 Filter=Ni Calibration= d-Cutoff= I/Ic(RIR)= Ref= Brauer, Esselborn. Z. Anorg. Allg. Chem., 309 151 (1961) Hexagonal - Powder Diffraction, P63/mmc (194) Z=2 mp= Cell=2.942x5.548 Pearson=hP4 (As Ni) Density(c)=8.390 Density(m)=8.66A Mwt=106.91 Vol=41.59 F(18)=3.7(0.179,27) Ref= Ibid. Strong Line: 2.31/X 2.74/8 1.87/8 0.85/8 1.49/8 1.47/8 1.01/8 0.78/8 1.30/7 0.95/7 NOTE: The composition Nb N0.99 is designated as $GD. O assigned because average $VD2$GU is 0.179. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 2.7400 80.0 30.0 0 0 2 32.655 16.327 0.1825 2.2931 2.5500 60.0 25.0 1 0 0 35.164 17.582 0.1961 2.4640 2.3070 100.0 45.0 1 0 1 39.010 19.505 0.2167 2.7235 1.8720 80.0 45.0 1 0 2 48.595 24.297 0.2671 3.3564 1.4870 75.0 53.0 1 0 3 62.398 31.199 0.3362 4.2254 1.4740 75.0 53.0 1 1 0 63.011 31.505 0.3392 4.2627 1.3740 25.0 19.0 68.196 34.098 0.3639 4.5729 1.2980 65.0 52.0 1 1 2 72.802 36.401 0.3852 4.8407 1.2740 15.0 12.0 2 0 0 74.402 37.201 0.3925 4.9319 1.2430 60.0 50.0 2 0 1 76.588 38.294 0.4023 5.0549 1.2110 20.0 17.0 78.999 39.499 0.4129 5.1884 1.1580 35.0 32.0 2 0 2 83.392 41.696 0.4318 5.4259 1.0480 40.0 40.0 2 0 3 94.614 47.307 0.4771 5.9954 1.0080 75.0 78.0 1 1 4 99.666 49.833 0.4960 6.2333 0.9660 15.0 16.0 2 1 0 105.763 52.882 0.5176 6.5043 0.9520 65.0 71.0 108.020 54.010 0.5252 6.6000 0.9380 15.0 17.0 2 0 4 110.409 55.204 0.5330 6.6985 0.9120 40.0 46.0 2 1 2 115.259 57.630 0.5482 6.8895 0.8660 20.0 24.0 125.613 62.807 0.5774 7.2554 0.8500 80.0 98.0 3 0 0 129.974 64.987 0.5882 7.3920 0.8370 40.0 50.0 2 0 5 133.936 66.968 0.5974 7.5068 0.8170 65.0 83.0 141.060 70.530 0.6120 7.6906 0.7940 35.0 46.0 151.920 75.960 0.6297 7.9133 0.7830 75.0 100.0 1 1 6 159.317 79.658 0.6386 8.0245 |
2楼2011-05-16 10:25:05