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【求助】急求Cu2o 的pdf卡片！用于做标准图谱的！急求谢谢！！！！！ 已有2人参与
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gyliu
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小木虫(金币+0.5):给个红包，谢谢回帖交流
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PDF#65-3288: QM=Calculated; d=Calculated; I=Calculated Copper Oxide Cu2 O Radiation=CuKa1 Lambda=1.54060 Filter= Calibration= d-Cutoff= I/Ic(RIR)=8.63 Ref= Calculated from NIST using POWD-12++ Cubic - (Unknown), Pn-3m (224) Z=2 mp= Cell=4.26 Pearson=cP6 (Ag2 O) Density(c)=6.146 Density(m)=6.090 Mwt=143.09 Vol=77.31 F(20)=999.9(.0003,20) Ref= M.Neuberger Z. Kristallogr., Kristallgeom., Kristallphys., Kristallchem., 77 169 (1931) Strong Line: 2.46/X 2.13/4 1.51/3 1.28/2 0.98/1 0.87/1 0.82/1 3.01/1 0.95/1 1.23/1 NOTE: N AL4552 3545 IB=Cu,O See PDF 01-077-0199. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 3.0123 5.3 4.3 1 1 0 2 29.632 14.816 0.1660 2.0859 2.4595 100.0 100.0 1 1 1 3 36.502 18.251 0.2033 2.5546 2.1300 35.3 40.8 2 0 0 4 42.401 21.201 0.2347 2.9499 1.7391 1.2 1.7 2 1 1 6 52.579 26.290 0.2875 3.6128 1.5061 28.6 46.7 2 2 0 8 61.518 30.759 0.3320 4.1717 1.4200 0.1 0.2 2 2 1 9 65.701 32.851 0.3521 4.4248 1.3471 0.3 0.5 3 1 0 10 69.751 34.875 0.3712 4.6641 1.2844 22.2 42.5 3 1 1 11 73.697 36.848 0.3893 4.8918 1.2298 4.8 9.6 2 2 2 12 77.565 38.783 0.4066 5.1093 1.1385 0.3 0.6 3 2 1 14 85.150 42.575 0.4392 5.5187 1.0650 2.9 6.7 4 0 0 16 92.650 46.325 0.4695 5.8997 1.0332 0.1 0.2 3 2 2 17 96.409 48.205 0.4839 6.0813 1.0041 0.1 0.2 4 1 1 18 100.196 50.098 0.4980 6.2576 0.9773 6.7 16.9 3 3 1 19 104.028 52.014 0.5116 6.4291 0.9526 5.0 12.9 4 2 0 20 107.926 53.963 0.5249 6.5961 0.9296 0.1 0.3 4 2 1 21 111.912 55.956 0.5379 6.7590 0.9082 0.1 0.3 3 3 2 22 116.013 58.006 0.5505 6.9180 0.8696 5.9 16.7 4 2 2 24 124.705 62.352 0.5750 7.2256 0.8355 0.1 0.3 4 3 1 26 134.437 67.219 0.5985 7.5207 0.8198 5.9 17.7 5 1 1 27 139.953 69.977 0.6099 7.6639 |
2楼2011-01-13 09:59:13
gyliu
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PDF#34-1354: QM=Intermediate; d=(Unknown); I=Film/Visual Copper Oxide Cu2 O Radiation=MoKa Lambda=0.710688 Filter= Calibration= d-Cutoff= I/Ic(RIR)= Ref= Kalliomaki, M. et al. Phys. Status Solidi, 56 K127 (1979) Cubic - (Unknown), Pn-3m (224) Z=2 mp= Cell=4.217 Pearson=cP6 (Ag2 O) Density(c)=6.337 Density(m)=8.80A Mwt=143.09 Vol=74.99 F(5)=9.3(0.067,8) Ref= Ibid. Strong Line: 2.43/X 2.12/X 1.49/8 1.27/5 2.98/3 0.00/1 0.00/1 0.00/1 0.00/1 0.00/1 NOTE: The X-ray samples were prepared from small crystals of optical quality and were studied in a diamond anvil cell under hydrostatic or quasi-hydrostatic pressure, the pressure was calibrated against a NaCl scale. Pattern at high pressure, 5.0 GPa. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 2.9780 25.0 17.0 1 1 0 2 29.981 14.990 0.1679 2.1099 2.4270 100.0 82.0 1 1 1 3 37.009 18.505 0.2060 2.5889 2.1200 100.0 93.0 2 0 0 4 42.611 21.305 0.2358 2.9638 1.4860 75.0 100.0 2 2 0 8 62.444 31.222 0.3365 4.2283 1.2740 50.0 78.0 3 1 1 11 74.402 37.201 0.3925 4.9319 |
3楼2011-01-13 10:00:27
gyliu
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PDF#05-0667: QM=Star(+); d=(Unknown); I=Diffractometer Cuprite, syn Cu2 +1 O (Violet red) Radiation=CuKa1 Lambda=1.5405 Filter=Ni Calibration= d-Cutoff= I/Ic(RIR)= Ref= Swanson, Fuyat. Natl. Bur. Stand. (U.S.), Circ. 539, II 23 (1953) Cubic - Powder Diffraction, Pn-3m (224) Z=2 mp= Cell=4.2696 Pearson=cP6 (Ag2 O) Density(c)=6.100 Density(m)=8.80A Mwt=143.09 Vol=77.83 F(13)=56.3(.0115,20) Ref= Restori, R., Schwarzenbach, D. Acta Crystallogr., Sec. B: Structural Science, 42 201 (1986) Strong Line: 2.47/X 2.14/4 1.51/3 1.29/2 3.02/1 1.23/1 0.98/1 0.95/1 0.87/1 0.82/1 NOTE: Sample prepared at NBS, Gaithersburg, Maryland, USA, by sintering CuCl and Na2 C O2 at ~800 C, then leaching with water and drying. See ICSD 38233 (PDF 01-077-0199); See ICSD 63281 (PDF 01-078-2076). Spectroscopic analysis: <1% Ca, Si; <0.1% Al, Mg; <0.01% Ag, B, Ba, Fe, Ti; <0.001% Mn, Pb, Sn. Pattern taken at 26 C. Opaque mineral optical data on specimen from Liskeard, Cornwall, England, UK. Pattern reviewed by Martin, K., McCarthy, G., North Dakota State Univ., Fargo, North Dakota, USA, ICDD Grant-in-Aid (1990). Agrees well with experimental and calculated patterns. Additional weak reflection [indicated by brackets] was observed. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 3.0200 9.0 7.0 1 1 0 2 29.554 14.777 0.1656 2.0805 2.4650 100.0 100.0 1 1 1 3 36.418 18.209 0.2028 2.5490 2.1350 37.0 43.0 2 0 0 4 42.297 21.149 0.2342 2.9429 1.7430 1.0 1.0 2 1 1 6 52.454 26.227 0.2869 3.6048 1.5100 27.0 44.0 2 2 0 8 61.344 30.672 0.3311 4.1611 1.3502 1.0 2.0 3 1 0 10 69.569 34.785 0.3703 4.6535 1.2870 17.0 33.0 3 1 1 11 73.526 36.763 0.3885 4.8820 1.2330 4.0 8.0 2 2 2 12 77.323 38.662 0.4055 5.0959 1.0674 2.0 5.0 4 0 0 16 92.380 46.190 0.4684 5.8864 0.9795 4.0 10.0 3 3 1 19 103.701 51.850 0.5105 6.4147 0.9548 3.0 8.0 4 2 0 20 107.558 53.779 0.5237 6.5806 0.8715 3.0 8.0 4 2 2 24 124.222 62.111 0.5737 7.2096 0.8216 3.0 9.0 5 1 1 27 139.284 69.642 0.6086 7.6475 |
4楼2011-01-13 10:01:26
5楼2011-01-13 11:10:07
