| 查看: 1780 | 回复: 4 | |||
[交流]
【求助】投acta cry e被拒，作者写的意见，我该如何解决他提的问题
|
|
各位大侠： 我的水平不高，写了篇文章投acta cry e被拒，编辑提了些意见，我不能解决，请各位大侠帮帮忙，谢谢！我还想问一下，投acta cry e可以更换编辑吗？谢谢！ 下面是编辑提的意见： The refinement has not fully converged and the number of L.S. was low. You should after each cycle change in the generated *.res the weighting scheme as suggested, to rename *res to *.ins and to repeat the refinement until the wighting scheme more or less converges to stable values. One again: There is a very short O…H…O hydrogen bond. It is wrong to restrain the pertinent distance O-H. All the description and the discussion of the structure is wrong! _publ_section_exptl_refinement ; Positional parameters of all the H atoms bonded to O and N atoms were calculated geometrically and were allowed to ride on the C atoms to which they are bonded. All H atoms had their displacement parameters constrained to be 1.2 (for those bonded to C atoms) or 1.5 (for those bonded to N and O atoms) times that of their hosts. O---H distances were refined with a restrained bond distance of 0.82 (1) \%A using DFIX command implemented in SHELXL97 (Sheldrick, 2008). ; This is a blunder! You should always consult the difference electron density map. If you had had done it you would have seen the position of the H atom involved in the short O…H…O bond. _publ_section_abstract ; The bisphosphonic acid group in the title compound, C~7~H~14~N~2~O~7~P~2~, has a strcture similar to zoledronic acid (ZL). ZL is a potent bone antiresorptive bisphosphonate drug having significant activity against several parasitic protozoa. EIHDP has inner-salt character, consisting of a negatively charged PO~3~ group and a positively charged N1 atom. The crystal packing is dominated by an extensive hydrogen bonding network. ; There is no PO3 group, rather alkylphosphate. ZL has nothing to do in Abstract because it is not a title structure. “inner salt” character: It is quite common that the parts of the molecules have a different charge. The most important features, such as the description of the H-bonding, is missing. phosphonate atom O7 is ionized and the H atom is transferred to atom N1, which adopts a tetrahedral geometry (Table 1). But O7 is an acceptor of the H-bond. Why is not ionized O5? In other words how can you determine the origin of the H atom attached to N? Please avoid using abbreviations: The PCP backbone I must partly apologize for one thing: Using a higher theta limit you the theta shell is not complete. I would suggest you to remeasure the structure again Even _diffrn_measured_fraction_theta_max 0.976 _diffrn_reflns_theta_full 25.00 is quite low. Your submission has been rejected twice. It would be pity if such a structure is lost in case of rejection because the short O…O hydrogen bond is quite interesting. |
回复此楼» 猜你喜欢
在MOF中，有没有羧基参加配位的情况
已经有2人回复
-
招2026年入学上海交通大学博士生，急！！！
已经有1人回复
-
无机化学论文润色/翻译怎么收费?
已经有279人回复
-
理论计算合作
已经有0人回复
-
求高校合作
已经有1人回复
-
27级无机化学申博自荐
已经有2人回复
-
Chemdraw免费软件
已经有0人回复
-
单晶结构解析，各类疑难晶体数据处理和答疑
已经有38人回复
-
这个水相反应有没有催化剂促进发生
已经有4人回复
-
Mn Me3TACN
已经有5人回复
» 本主题相关价值贴推荐，对您同样有帮助:
- 已被受理单位审核通过暂无处理意见
已经有14人回复
- 征询大家对CSC政策的意见
已经有5人回复
- 怒了，Acta Mater 审稿意见
已经有23人回复
- 期刊选择的问题 script 和acta
已经有6人回复
- 给Acta E 投稿，汇款问题，编辑说少了15美元？什么意思啊？
已经有14人回复
- Microchim Acta杂志状态一直保持with editor差不多十天了，是不是很可能被拒啊？急！
已经有10人回复
- 投Acta E 时提示出现Non-printable ASCII character，是把摘要comment都写进出现的
已经有5人回复
- acta E 想弄俩通讯作者，怎么弄呢？
已经有6人回复
- 投acta，审稿人给了较正面的意见，但是编辑却给据了，苍天啦，大地啦
已经有19人回复
- 英文写出来了，老师没提意见，论文不知如何修改，不敢投啊？
已经有6人回复
- 【求助】请教Acta Biomaterialia投稿问题
已经有8人回复
- Analytical Chimica Acta 投稿问题
已经有13人回复
- 【请教】投稿acta e 后被拒，修改后再投稿...
已经有11人回复
marise
木虫 (小有名气)
- 应助: 17 (小学生)
- 金币: 2303.2
- 红花: 1
- 帖子: 257
- 在线: 71.4小时
- 虫号: 434856
- 注册: 2007-08-19
- 性别: MM
- 专业: 英语翻译
2楼2010-08-23 16:40:25
gohappy
铜虫 (正式写手)
- 应助: 14 (小学生)
- 金币: 4763.4
- 散金: 59
- 红花: 1
- 帖子: 843
- 在线: 425.6小时
- 虫号: 265745
- 注册: 2006-07-15
- 专业: 无机材料化学
3楼2010-08-23 16:49:56
xiaochong98
木虫 (职业作家)
- CMEI: 1
- 应助: 208 (大学生)
- 金币: 19217.6
- 散金: 20
- 红花: 16
- 帖子: 4720
- 在线: 668小时
- 虫号: 71782
- 注册: 2005-06-01
- 性别: GG
- 专业: 生物化学
4楼2010-08-23 19:02:27
5楼2010-08-24 09:31:50
20