1.我烧催化剂时,由于同事们也要用炉子,炉子有时没完全冷却到室温,这影响吗? I am sure it will influence.
2.我的电流速率快到10,是不是电流速率太大了,通过实验,烧成灰黑色的催化剂效果明显不好,怎样避免这种情况呢?
You should use the programmed-temperature to controll the rising speed.
浸渍法一般用搅拌 to get homogeneous phase.
有时烧的催化剂呈现灰黑色,有时是土的颜色,There are two possible resons:
First, it is due to the oven without controlling termperature exactly.
Second, it is due to the aggregation on the surface.