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13CNMR(101MHz,MeOD)δ20.7,25.6,28.7,43.2,64.4,69.3,71.6,71.7,74.9,75.1,75.3,75.5,75.9,78.7,96.7,97.0,97.6,105.7,105.8,113.5,118.6,120.5,120.7,121.1,121.2,122.3,130.8,132.6,132....

13CNMR(101MHz,D2O)δ24.0,26.4,41.5,49.0,60.5,60.7,69.1,69.5,72.6,73.2,75.5,75.6,76.2,76.3,96.6,97.3,98.1,98.2,104.6,117.8,120.2,120.7,131.3,134.1,140.8,148.3,153.2,169.0.

13CNMR(101MHz,DMSO)δ13.9,31.8,45.8,61.6,70.5,73.6,76.9,77.6,79.1,96.3,99.2,112.1,113.6,119.9,120.3,121.5,146.3,150.0,151.5,168.7,169.8.

13CNMR(101MHz,MeOD)δ60.7,61.1,61.7,62.3,63.3,64.8,68.5,70.2,70.6,70.8,71.4,72.0,72.4,72.6,73.1,73.4,73.5,73.7,74.9,75.1,76.7,76.9,77.2,77.3,82.4,82.8,93.1,96.9,100.9,104.6.

13CNMR(101MHz,MeOD)δ11.5,19.4,19.4,29.9,40.3,41.0,45.1,50.4,60.6,62.2,69.4,71.6,71.8,72.0,73.2,73.8,76.3,77.2,78.1,95.7,96.4,104.9,113.9,121.0,121.1,125.1,125.8,143.3,149.5,...

13CNMR(101MHz,MeOD)δ11.5,19.1,19.4,29.4,29.9,40.3,41.1,45.1,50.4,60.8,62.0,69.5,69.5,71.0,71.5,72.4,73.8,76.3,77.3,95.8,96.1,104.7,113.9,121.1,121.6,124.8,125.0,143.5,149.5,...

13CNMR(101MHz,CDCl3)δ7.4,9.5,17.6,18.6,18.9,21.4,21.6,27.1,27.3,27.7,36.7,38.6,43.4,45.3,47.0,48.6,52.4,55.7,56.6,67.6,69.3,70.7,82.8,84.7,105.9,120.9,127.8,129.9,154.4,195.4,...

13CNMR(101MHz,MeOD)δ12.8,12.8,19.4,20.5,20.7,20.7,20.7,20.8,20.9,31.1,41.4,41.5,42.2,42.3,46.3,51.8,63.2,63.9,69.3,71.7,72.6,73.2,74.3,75.0,75.1,76.2,96.9,97.0,97.4,97.6,115.0...

13CNMR(101MHz,D2O)δ28.5,36.7,42.3,43.5,63.3,63.9,67.6,69.5,71.4,74.1,75.4,75.7,75.9,76.2,95.9,96.5,96.9,98.1,115.5,120.2,120.8,131.9,133.0,145.9,180.5LF-63谢谢

13CNMR(101MHz,MeOD)δ69.7,69.9,70.1,70.2,70.3,70.4,71.1,71.6,71.9,72.2,72.3,72.6,72.9,73.1,73.4,74.4,74.7,76.3,76.4,78.1,82.0,83.2,92.4,92.5,96.6.

58.3,61.3,64.8,69.2,69.4,71.6,73.0,74.8,75.1,75.6,96....121.3,121.4,121.9,122.4,129.8,129.8,132.2,132.5,133.2,133.2,146.8,146.9,151.2,153.2,167.3,169.5,169.5,171.1,171.3.LF-23

13CNMR(101MHz,MeOD)δ14.2,19.9,23.6,30.6,32.9,35.7,44.0,62.6,80.3,95.0,96.2,100.1,103.8,116.3,116.9,123.2,128.9,129.3,158.8,162.6,164.7,165.9,166.2,168.3,183.8,197.6

14.2,18.4,22.7,29.7,39.4,51.8,58.4,60.0,62.2,62.9,69.7,72.9,76.0,76.4,77.2,96.9,98.8,110.2,133.9,168.8，溶剂氯仿

13CNMR(101MHz,)δ11.6,18.2,30.9,31.5,35.7,44.0,50.8,51.5,53.5,69.8,96.2,103.1,108.7,120.7,133.1,152.5,167.4,201.6

120.84,120.51,120.17,119.34,114.64,114.04,113.45,113.14,111.55,111.32,105.93,105.74,103.01,100.07,99.63,97.93,97.76,97.55,96.82,79.99,78.16,77.89,77.78,77.59,75.63,75.28,74.75,...