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单晶有不少错误解析困难，请求帮助，谢谢！

作者 jinshanli: 来源: 小木虫 200 4 举报帖子

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测出来的单晶有不少错误，说是单晶无序，请各位单晶解析高手帮忙解析一下，谢谢啦！
主要想确定结构中标红的两个基团相对构型，是顺式还是反式的，非常感谢！

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羊倌

test-name_ALERT_alert-type_alert-level.
Click on the hyperlinks for more details of the test.
Alert level A
EXPT005_ALERT_1_A  _exptl_crystal_description is missing
         Crystal habit description.
         The following tests will not be performed.
         CRYSR_01
DIFF003_ALERT_1_A  _diffrn_measurement_device_type is missing
         Diffractometer make and type. Replaces _diffrn_measurement_type.
PLAT183_ALERT_1_A Missing _cell_measurement_reflns_used Value ....    Please Do !
PLAT184_ALERT_1_A Missing _cell_measurement_theta_min Value ......    Please Do !
PLAT185_ALERT_1_A Missing _cell_measurement_theta_max Value ......    Please Do !
PLAT699_ALERT_1_A Missing _exptl_crystal_description Value .......    Please Do !
Alert level C
PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings  Differ    Please Check
PLAT043_ALERT_1_C Calculated and Reported Mol. Weight Differ by ..    2.02 Check
PLAT052_ALERT_1_C Info on Absorption Correction Method Not Given    Please Do !
PLAT053_ALERT_1_C Minimum Crystal Dimension Missing (or Error) ...    Please Check，
羊倌

test-name_ALERT_alert-type_alert-level.
Click on the hyperlinks for more details of the test.
Alert level A
EXPT005_ALERT_1_A  _exptl_crystal_description is missing
         Crystal habit description.
         The following tests will not be performed.
         CRYSR_01
DIFF003_ALERT_1_A  _diffrn_measurement_device_type is missing
         Diffractometer make and type. Replaces _diffrn_measurement_type.
PLAT183_ALERT_1_A Missing _cell_measurement_reflns_used Value ....    Please Do !
PLAT184_ALERT_1_A Missing _cell_measurement_theta_min Value ......    Please Do !
PLAT185_ALERT_1_A Missing _cell_measurement_theta_max Value ......    Please Do !
PLAT699_ALERT_1_A Missing _exptl_crystal_description Value .......    Please Do !
Alert level C
PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings  Differ    Please Check
PLAT043_ALERT_1_C Calculated and Reported Mol. Weight Differ by ..    2.02 Check
PLAT052_ALERT_1_C Info on Absorption Correction Method Not Given    Please Do !
PLAT053_ALERT_1_C Minimum Crystal Dimension Missing (or Error) ...    Please Check
我想更懂你29

链接: https://pan.baidu.com/s/1Zb4qaDgj1s04-5GCbGqxLw 提取码: yw9j
无序与否并不影响两个目标基团位置的判断
HDJ_Tokyo

附件仅供参考。